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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22931 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-43 Analysis Batch: 720-22968 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22931 Lab File ID: 062107011.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.02 g <br /> Date Analyzed: 06/21/2007 1914 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1357 Injection Volume: <br /> MSD Lab Sample ID: 720-9514-43 Analysis Batch: 720-22968 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22931 Lab File ID: 062107012.D <br /> Dilution: 1.0 Initial Weight/Volume: 30.11 g <br /> Date Analyzed: 06/21/2007 1941 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1357 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 72 72 21 - 133 1 35 <br /> Acenaphthene 70 69 40- 145 2 35 <br /> Acenaphthylene 77 74 33- 145 4 35 <br /> Fluorene 76 74 50- 121 3 35 <br /> Phenanthrene 80 78 10- 130 3 35 <br /> Anthracene 70 69 27- 133 3 35 <br /> Benzo[a]anthracene 88 86 33- 143 3 35 <br /> Chrysene 72 70 17- 168 3 35 <br /> Benzo[a]pyrene 75 75 17- 163 1 35 <br /> Benzo[b]fluoranthene 86 87 24- 159 1 35 <br /> Benzo[k]fluoranthene 69 81 11 - 162 16 35 <br /> Benzo[g,h,i]perylene 78 79 9-219 1 35 <br /> Indeno[1,2,3-cd]pyrene 81 83 9- 171 1 35 <br /> Fluoranthene 80 78 26- 137 2 35 <br /> Pyrene 84 82 52- 115 3 35 <br /> Dibenz(a,h)anthracene 71 71 52- 115 0 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 70 71 30- 115 <br /> Terphenyl-d14 88 86 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 191 of 222 06/25/2007 <br />