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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22947 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-48 Analysis Batch: 720-23002 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22947 Lab File ID: 062207018.D <br /> Dilution: 2.0 Initial Weight/Volume: 30.13 g <br /> Date Analyzed: 06/22/2007 1851 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1601 Injection Volume: <br /> MSD Lab Sample ID: 720-9514-48 Analysis Batch: 720-23002 Instrument ID: Latest Chemstation <br /> Client Matrix: Solid Prep Batch: 720-22947 Lab File ID: 062207019.D <br /> Dilution: 2.0 Initial Weight/Volume: 30.35 g <br /> Date Analyzed: 06/22/2007 1917 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1601 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 60 59 21 - 133 2 35 <br /> Acenaphthene 61 63 40- 145 2 35 <br /> Acenaphthylene 67 65 33- 145 4 35 <br /> Fluorene 66 64 50- 121 3 35 <br /> Phenanthrene 64 65 10- 130 1 35 <br /> Anthracene 61 62 27- 133 1 35 <br /> Benzo[a]anthracene 71 70 33- 143 1 35 <br /> Chrysene 65 65 17- 168 0 35 <br /> Benzo[a]pyrene 67 69 17- 163 2 35 <br /> Benzo[b]fluoranthene 72 70 24- 159 4 35 <br /> Benzo[k]fluoranthene 65 67 11 - 162 3 35 <br /> Benzo[g,h,i]perylene 58 60 9-219 2 35 <br /> Indeno[1,2,3-cd]pyrene 69 69 9- 171 1 35 <br /> Fluoranthene 68 71 26- 137 2 35 <br /> Pyrene 73 77 52- 115 5 35 <br /> Dibenz(a,h)anthracene 57 57 52- 115 0 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 69 57 30- 115 <br /> Terphenyl-d14 77 77 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 195 of 222 06/25/2007 <br />