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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Matrix Spike/ Method: 8270C <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22952 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-83 Analysis Batch: 720-22989 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22952 Lab File ID: c:\saturnws\epdata\data\2 <br /> Dilution: 1.0 Initial Weight/Volume: 30.05 g <br /> Date Analyzed: 06/22/2007 1625 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1918 Injection Volume: <br /> MSD Lab Sample ID: 720-9514-83 Analysis Batch: 720-22989 Instrument ID: Sat 2K2 <br /> Client Matrix: Solid Prep Batch: 720-22952 Lab File ID: c:\saturnws\epdata\data\20 <br /> Dilution: 1.0 Initial Weight/Volume: 30.02 g <br /> Date Analyzed: 06/22/2007 1654 Final Weight/Volume: 1 mL <br /> Date Prepared: 06/21/2007 1918 Injection Volume: <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Naphthalene 58 54 21 - 133 6 35 <br /> Acenaphthene 58 54 40- 145 7 35 <br /> Acenaphthylene 61 53 33- 145 14 35 <br /> Fluorene 65 60 50- 121 8 35 <br /> Phenanthrene 58 54 10- 130 7 35 <br /> Anthracene 61 59 27- 133 4 35 <br /> Benzo[a]anthracene 64 65 33- 143 2 35 <br /> Chrysene 65 63 17- 168 3 35 <br /> Benzo[a]pyrene 62 63 17- 163 1 35 <br /> Benzo[b]fluoranthene 70 71 24- 159 2 35 <br /> Benzo[k]fluoranthene 60 63 11 - 162 5 35 <br /> Benzo[g,h,i]perylene 64 65 9-219 2 35 <br /> Indeno[1,2,3-cd]pyrene 69 71 9- 171 3 35 <br /> Fluoranthene 62 58 26- 137 7 35 <br /> Pyrene 66 64 52- 115 2 35 <br /> Dibenz(a,h)anthracene 71 73 52- 115 3 35 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> 2-Fluorobiphenyl 59 54 30- 115 <br /> Terphenyl-d14 65 65 18- 137 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 198 of 222 06/25/2007 <br />