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Quality Control Results <br /> Client: Geomatrix Consultants Inc. Job Number: 720-9514-1 <br /> Matrix Spike/ Method: 8015B <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22941 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-65 Analysis Batch: 720-23000 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-22941 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.03 g <br /> Date Analyzed: 06/22/2007 0312 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/21/2007 1450 Injection Volume: <br /> Column ID: PRIMARY <br /> MSD Lab Sample ID: 720-9514-65 Analysis Batch: 720-23000 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-22941 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.41 g <br /> Date Analyzed: 06/22/2007 0338 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/21/2007 1450 Injection Volume: <br /> Column ID: PRIMARY <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Diesel Range Organics[C10-C28] 84 76 50- 130 10 30 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> o-Terphenyl 85 80 46- 105 <br /> Matrix Spike/ Method: 8015B <br /> Matrix Spike Duplicate Recovery Report- Batch: 720-22941 Preparation: 3550B <br /> MS Lab Sample ID: 720-9514-48 Analysis Batch: 720-23000 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-22941 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.02 g <br /> Date Analyzed: 06/22/2007 0550 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/21/2007 1450 Injection Volume: <br /> Column ID: PRIMARY <br /> MSD Lab Sample ID: 720-9514-48 Analysis Batch: 720-23000 Instrument ID: HP DRO5 <br /> Client Matrix: Solid Prep Batch: 720-22941 Lab File ID: N/A <br /> Dilution: 1.0 Initial Weight/Volume: 30.28 g <br /> Date Analyzed: 06/22/2007 0616 Final Weight/Volume: 5 mL <br /> Date Prepared: 06/21/2007 1450 Injection Volume: <br /> Column ID: PRIMARY <br /> % Rec. <br /> Analyte MS MSD Limit RPD RPD Limit MS Qual MSD Qual <br /> Diesel Range Organics[C10-C28] 127 98 50- 130 19 30 <br /> Surrogate MS% Rec MSD % Rec Acceptance Limits <br /> o-Terphenyl 71 77 46- 105 <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> STL San Francisco Page 204 of 222 06/25/2007 <br />