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cbCurtis &Tompkins, Ltd, <br /> CASE NARRATIVE <br /> Laboratory number: 218019 <br /> Client: Oneida Total Integrated Enterprises <br /> Project: 2009069 <br /> Location: CA ARNG - LODI <br /> Request Date: 01/28/10 <br /> Samples Received: 01/28/10 <br /> Pesticides (EPA 8081A) : <br /> 02/05/10 17 :01; average CCV drift met method requirements. <br /> Matrix spikes were not performed for this analysis in batch 159701 due to <br /> insufficient sample amount. <br /> No other analytical problems were encountered. <br /> PCBs (EPA 8082) : <br /> All samples underwent sulfuric acid cleanup using EPA Method 3665A. <br /> All samples underwent sulfur cleanup using the copper option in EPA Method <br /> 3660B. <br /> No analytical problems were encountered. <br /> Metals (EPA 6010B and EPA 7471A) : <br /> Mercury was detected between the MDL and the RL in the method blank for batch <br /> 159626; this analyte was not detected in the sample at or above the RL. <br /> No other analytical problems were encountered. <br /> Moisture (ASTM D2216/CLP) : <br /> No analytical problems were encountered. <br /> ChlorophenoxV Herbicides (EPA 8151) : <br /> Cal Science in Garden Grove, CA performed the analysis (not NELAP certified) . <br /> Please see the Cal Science case narrative. <br /> Page 2 of 2 <br /> 33.o <br /> 3 of 295 <br />