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CURTIS & TOMPKINS INITIAL CALIBRATION FOR 218019 MSVOA Soil : EPA 8260B Inst : MSVOAI2 Name : 8260GX12 Calnum : 880051023001 Date : 04-FEB-2010 20 : 13 Type SOIL Units : ug/L X Axis : R Level File Seqnum Sample ID Analyzed Stds Ll lb412 880051023012 2.3PPB 04-FEB-2010 20:13 513953 (20000X), 513954 (20000X), 513956 (20000X), 513687 (5000X) L2 lb413 880051023013 SPPB 04-FEB-2010 20:47 513953 (10000X), 513954 (10000X), 513956 (10000X), 513687 (5000X) L3 lb414 880051023014 i0PPB 04-FEB-2010 21:20 513953 (5000X), 513954 (5000X), 513956 (5000X), 513687 (5000X) L4 lb415 880051023015 20PPB 04-FEB-2010 21:54 513952 (25000X), 513796 (25000X), 513556 (25000X), 513687 (5000X) LS lb416 880051023016 30PPB 04-FEB-2010 22:28 513952 (10000X), 513796 (10000X), 513556 (10000X), 513687 (5000X) L6 lb417 880051023017 60PPB 04-FEB-2010 23:01 513952 (8333X), 513796 (8333X), 513556 (8333X), 513687 (5000X) L7 lb418 880051023018 73PPB 04-FEB-2010 23:35 513952 (6667X), 513796 (6667X), 513556 (6667X), 513687 (5000X) L8 lb419 880051023019 100PPB 03-FEB-2010 00:09 513952 (5000X), 513796 (5000X), 513556 (5000X), 513687 (5000X) L9 lb420 880051023020 200PPB 05-FEB-2010 00:43 513952 (2500X), 513796 (2500X), 513556 (2500X), 513687 (5000X) r^2 Max Min Min Analyte Ll L2 L3 L4 L5 L6 L7 L8 L9 Type a0 al a2 Avg %RSD %RSD RF r^2 Fig Freon 12 0.6925 0.6552 0.7047 0.7768 0.6798 0.6760 0.8185 0.8470 AVRG 1.36742 0.7313 10 15 0.05 0.99 Chloromethane 1.6068m 1.5332 1.6985m 1.6956m 1.5949m 1.7067m 1.5906 1.6386m AVRG 0.61233 1.6331 4 15 0.10 0.99 Vinyl Chloride 0.9089 0.8679 0.9435 1.0000 0.9036 0.9959 1.0054 1.0682 AVRG 1.03986 0.9617 7 15 0.05 0.99 Bromomethane 0.4631 0.4144 0.4362 0.4135 0.4029 0.4177 0.4243 0.4481 AVRG 2.33900 0.4275 5 15 0.05 0.99 Chloroethane 0.4629 0.4321 0.4883 0.5056 0.4817 0.5233 0.5145 0.5512 AVRG 2.02041 0.4949 8 15 0.05 0.99 Trichlorofluoromethane 0.7569 0.7053 0.7944 0.8038 0.6958 0.7744 0.8477 0.9133 AVRG 1.27153 0.7865 9 15 0.05 0.99 Acetone 0.2941 0.3020 0.2610 0.2628 0.2797 0.2566 0.2499 AVRG 3.67237 0.2723 7 15 0.05 0.99 Freon 113 0.4409 0.4562 0.4496 0.4759 0.4719 0.4989 0.4646 0.4759 AVRG 2.14255 0.4667 4 15 0.05 0.99 1,1-Dichloroethene 0.3861 0.4010 0.3974 0.4286 0.4136 0.4392 0.4026 0.4161 AVRG 2.43561 0.4106 4 15 0.05 0.99 Methylene Chloride 0.4869 0.5000 0.4827 0.5173 0.4909 0.5086 0.4706 0.4829 AVRG 2.03046 0.4925 3 15 0.05 0.99 Carbon Disulfide 1.6329 1.6597 1.7162 1.8024 1.7323 1.8079 1.6509 1.6696 AVRG 0.58514 1.7090 4 15 0.05 0.99 MTBE 1.6013 1.4851 1.5667 1.6817 1.6263 1.7156 1.6030 1.5860 AVRG 0.62181 1.6082 4 15 0.05 0.99 trans-1,2-Dichloroethene 0.4537 0.4417 0.4601 0.4802 0.4627 0.4842 0.4411 0.4487 AVRG 2.17842 0.4590 4 15 0.05 0.99 Vinyl Acetate 1.4267 1.5519 1.6437 1.7774 1.7349 1.8426 1.7590 1.7447 AVRG 0.59343 1.6851 8 15 0.05 0.99 1,1-Dichloroethane 1.0427 1.0801 1.0924 1.1593 1.1149 1.1733 1.0789 1.1119 AVRG 0.90359 1.1067 4 15 0.10 0.99 2-Butanone 0.3947 0.3514 0.3663 0.4025 0.3945 0.4184 0.4074 0.4062 AVRG 2.54661 0.3927 6 15 0.05 0.99 2,2-Dichloropropane 0.8035 0.8403 0.8629 0.8973 0.8685 0.9048 0.8271 0.8404 AVRG 1.16879 0.8556 4 15 0.05 0.99 cis-1,2-Dichloroethene 0.4905 0.4958 0.5249 0.5566 0.5317 0.5600 0.5186 0.5247 AVRG 1.90349 0.5254 5 15 0.05 0.99 Chloroform 0.8970 0.8996 0.9202 0.9710 0.9243 0.9632 0.8902 0.8955 AVRG 1.08681 0.9201 3 15 0.05 0.99 Bromochloromethane 0.2403 0.2204 0.2290 0.2407 0.2286 0.2393 0.2226 0.2160 AVRG 4.35506 0.2296 4 15 0.05 0.99 1,1,1-Trichloroethane 0.7715 0.7677 0.7676 0.8135 0.8015 0.8259 0.7615 0.7888 AVRG 1.27026 0.7872 3 15 0.05 0.99 1,1-Dichloropropene 0.4543 0.4852 0.4856 0.5325 0.5065 0.5358 0.4882 0.5010 AVRG 2.00548 0.4986 5 15 0.05 0.99 Carbon Tetrachloride 0.4252 0.4419 0.4331 0.4703 0.4568 0.4752 0.4374 0.4440 AVRG 2.23226 0.4480 4 15 0.05 0.99 1,2-Dichloroethane 0.5076 0.5074 0.5322 0.5757 0.5353 0.5633 0.5229 0.5255 AVRG 1.87353 0.5338 5 15 0.05 0.99 Page 1 of 6 880051023001 54 of 295