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CURTIS & TOMPKINS INITIAL CALIBRATION FOR 218019 PEST Soil : EPA 8081A Inst : GC21 Name : gc21 608 340 Calnum : 249490441002 Date : 06-DEC-2009 17 : 36 Units : pg/uL Level File Seqnum Sample TD Analyzed Stds L1 340_011 249490441011 PEST 1 06-DEC-2009 17:36 512604 L2 340_012 249490441012 PEST_2 06-DEC-2009 17:58 512605 L3 340_013 249490441013 PEST_3 06-DEC-2009 18:19 512606 L4 340_014 249490441014 PEST_4 06-DEC-2009 18:41 513470 L5 340_013 249490441015 PESTS 06-DEC-2009 19:02 512608 L6 340_016 249490441016 PEST_6 06-DEC-2009 19:24 512609 L7 340_017 249490441017 PEST_7 06-DEC-2009 19:45 512610 r^2 Analyte h Ll L2 L3 L4 L5 L6 L7 Type X a0 al a2 Avg %RSD MnR^2 MxRSD Flg alpha-BHC A 4489.0 4115.6 3131.2 5163.6 5509.8 7255.3 QUAD A -2000.1 3660.22 72.99042 4944.1 0.998 0.990 20 gamma-BHC A 4068.0 3793.0 2929.4 4701.4 5054.5 6471.4 QUAD A -2316.1 3517.45 60.28858 4502.9 0.998 0.990 20 beta-BHC A 1887.5 1511.0 1145.1 1424.4 1404.3 1709.8 QUAD A 1421.03 1037.92 12.88842 1513.7 0.999 0.990 20 delta-BHC A 4883.5 3960.8 2924.1 4571.2 4754.2 6026.9 QUAD A -200.49 3340.77 54.04292 4520.1 0.998 0.990 20 Heptachlor A 3728.0 3419.0 2621.7 4553.3 4816.3 5557.1 QUAD A -5707.7 4072.66 32.34941 4115.9 0.996 0.990 20 Aldrin A 3658.0 3514.4 2665.0 4980.9 5275.3 5671.4 QUAD A -9306.1 4946.66 18.72483 4294.2 0.994 0.990 20 Heptachlor epoxide A 3314.5 3116.8 2373.4 4122.3 4346.3 4705.4 QUAD A -6318.2 4001.58 16.98175 3663.1 0.995 0.990 20 gamma-Chlordane A 3246.5 3109.8 2331.3 4143.4 4395.2 4892.9 QUAD A -6190.1 3902.31 22.66858 3686.5 0.995 0.990 20 alpha-Chlordane A 3093.5 2893.8 2193.8 3879.2 4119.0 4643.6 QUAD A -5535.7 3592.68 23.58192 3470.5 0.996 0.990 20 4,4'-DDE A 2550.3 2571.7 2157.4 4140.8 4138.4 3892.2 QUAD A -21626 4715.59 -5.86310 3241.8 0.990 0.990 20 Endosulfan T A 3092.5 2892.0 2196.2 3712.3 3947.4 4477.1 QUAD A -4546.7 3383.78 23.99823 3386.3 0.996 0.990 20 Dieldrin A 3351.5 3445.8 2795.9 4721.7 4634.9 3757.9 2480.1 QUAD A -19031 5482.88 -14.5623 3598.2 0.993 0.990 20 Endrin A 2733.5 2696.7 2186.1 3900.8 3832.4 3392.6 2280.2 QUAD A -21743 4794.36 -12.0117 3003.2 0.995 0.990 20 4,4'-DDD A 1916.3 1834.7 1443.2 2737.6 2815.8 3025.8 QUAD A -10638 2722.66 4.221610 2295.6 0.994 0.990 20 Endosulfan TT A 3072.8 2916.1 2274.8 3883.5 3888.2 3519.3 QUAD A -16137 4429.00 -7.29656 3259.1 0.991 0.990 20 4,4'-DDT A 2142.8 2111.1 1654.4 3197.3 3223.6 3168.2 QUAD A -14847 3477.12 -1.44570 2582.9 0.991 0.990 20 Endrin aldehyde A 2312.3 2030.3 1503.5 2614.7 2641.1 2765.3 QUAD A -7379.7 2575.95 2.740536 2311.2 0.994 0.990 20 Methoxychlor A 833.35 967.96 862.75 1198.7 1085.9 808.84 QUAD A -24535 1503.23 -1.28467 959.59 0.991 0.990 20 Endosulfan sulfate A 2424.5 2185.0 1646.8 2896.8 2942.9 3123.7 QUAD A -8686.1 2838.64 3.840203 2536.6 0.994 0.990 20 TCMX A 2275.0 2265.4 1688.2 2616.7 2627.0 3572.7 3822.3 QUAD A -17681 3140.49 3.945072 2695.3 0.997 0.990 20 Decachlorobiphenyl A 1435.0 1405.8 1084.7 1745.3 1784.1 2388.3 2255.9 QUAD A -16066 2390.20 -0.19178 1728.4 0.994 0.990 20 alpha-BHC B 4144.5 3801.2 2834.0 3769.9 3780.0 3991.7 4112.6 LTNR R 1.51558 2.41E-4 3776.3 0.999 0.990 20 gamma-BHC B 3529.0 3168.2 2375.7 3089.7 3112.0 3270.0 3433.5 LTNR R 1.67238 2.89E-4 3139.7 0.999 0.990 20 beta-BHC B 1597.0 1629.0 1237.1 1699.9 1491.1 1781.5 1667.8 LTNR R 0.78481 5.89E-4 1586.2 0.997 0.990 20 delta-BHC B 2795.5 2176.8 1612.6 2162.3 2045.1 2270.4 2388.4 LTNR R 1.84027 4.15E-4 2207.3 0.998 0.990 20 Heptachlor B 4919.0 4358.4 3272.3 4203.4 4550.5 4707.6 4667.6 LTNR R 1.16667 2.11E-4 4382.7 0.999 0.990 20 Page 1 of 4 249490441002 76 of 295