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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC21 Run Name : PEST_4 IDF : 1 . 0 Seqnum : 240050803016 File : 03516 Time : 04-FEB-2010 21 : 35 Cal : 249490441002 Caldate : 06-5EC-2009 Standards : 513887 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 4944.1 5294.8 20.00 20.83 pg/uL 4 15 gamma-BHC A 4502. 9 4721.7 20.00 20.38 pg/uL 2 15 beta-BHC A 1513.7 1363. 6 20.00 19. 96 pg/uL 0 15 delta-BHC A 4520.1 3901.8 20.00 18.11 pg/uL -9 15 Heptachlor A 4115. 9 4890.0 20.00 21. 68 pg/uL 8 15 Aldrin A 4294.2 5732. 6 20.00 23.05 pg/uL 15 15 Heptachlor epoxide A 3663.1 4711.2 20.00 22. 90 pg/uL 15 15 gamma-Chlordane A 3686.5 4603.5 20.00 22.29 pg/uL 11 15 alpha-Chlordane A 3470.5 4360.8 20.00 22.50 pg/uL 12 15 4,4'-DDE A 3241.8 4308.5 40.00 43.48 pg/uL 9 15 Endosulfan I A 3386.3 4217.3 20.00 22. 64 pg/uL 13 15 Dieldrin A 3598.2 5686.0 40.00 52.19 pg/uL 30 15 c+ *** Endrin A 3003.2 3801.8 40.00 40.33 pg/uL 1 15 4,4'-DDD A 2295. 6 2394. 6 40.00 36. 97 pg/uL -8 15 Endosulfan II A 3259.1 4766.3 40.00 50. 97 pg/uL 27 15 c+ *** 4,4'-DDT A 2582. 9 3085.0 40.00 40.44 pg/uL 1 15 Endrin aldehyde A 2311.2 2911. 9 40.00 45.85 pg/uL 15 15 Methoxychlor A 959.59 1317.3 200.0 241.4 pg/uL 21 15 c+ *** Endosulfan sulfate A 2536. 6 3001.1 40.00 42.86 pg/uL 7 15 TCMX A 2695.3 2730.7 40.00 38.54 pg/uL -4 15 Decachlorobiphenyl A 1728.4 1804.0 40.00 37.02 pg/uL -7 15 alpha-BHC B 3776.3 3557.5 20.00 18. 65 pg/uL -7 15 gamma-BHC B 3139.7 3114.3 20.00 19. 67 pg/uL -2 15 beta-BHC B 1586.2 1443.2 20.00 17.77 pg/uL -11 15 delta-BHC B 2207.3 2438. 6 20.00 22.10 pg/uL 10 15 Heptachlor B 4382.7 3786.8 20.00 17.18 pg/uL -14 15 Aldrin B 3513.3 3233.8 20.00 18.34 pg/uL -8 15 Heptachlor epoxide B 3041.4 2854.4 20.00 18.85 pg/uL -6 15 gamma-Chlordane B 2994.3 3230.1 20.00 21.57 pg/uL 8 15 alpha-Chlordane B 2774.5 2625.7 20.00 19.07 pg/uL -5 15 4,4'-DDE B 2183.4 2421.5 40.00 43. 61 pg/uL 9 15 Endosulfan I B 2888.4 2687.0 20.00 18. 93 pg/uL -5 15 Dieldrin B 3431.8 2972.8 40.00 34.57 pg/uL -14 15 Endrin B 1575.4 1647.4 40.00 41.02 pg/uL 3 15 4,4'-DDD B 1326.5 1775. 6 40.00 48.56 pg/uL 21 15 c+ *** Endosulfan II B 3292.5 2628.1 40.00 34.20 pg/uL -14 15 4,4'-DDT B 1907.5 1914.2 40.00 39.49 pg/uL -1 15 Endrin aldehyde B 2482.0 1989.5 40.00 33.15 pg/uL -17 15 c- *** Methoxychlor B 615. 91 784. 65 200.0 231.7 pg/uL 16 15 c+ *** Endosulfan sulfate B 2188.2 1757. 9 40.00 32. 98 pg/uL -18 15 c- *** TCMX B 1823. 9 1944.4 40.00 39.34 pg/uL -2 15 Decachlorobiphenyl B 1819.4 1755. 9 40.00 38. 60 pg/uL -3 15 Average EPA 8081A A (n=23) 11 15 Average EPA 8081A B (n=23) 9 15 TFB 02/04/10 : Corrected automatically drawn baseline. average ICAL %RSD out (A) Page 1 0' 2 240050803016 94 of 295