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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC21 Run Name : PEST_3 IDF : 1 . 0 Seqnum : 240050803022 File : 03522 Time : 05-FEB-2010 00 : 12 Cal : 249490441002 Caldate : 06-5EC-2009 Standards : 513886 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 4944.1 4752.1 10.00 11.08 pg/uL 11 15 gamma-BHC A 4502. 9 4278. 9 10.00 10.82 pg/uL 8 15 beta-BHC A 1513.7 1463.7 10.00 11.18 pg/uL 12 15 delta-BHC A 4520.1 3787.7 10.00 9.834 pg/uL -2 15 Heptachlor A 4115. 9 3774.0 10.00 9.891 pg/uL -1 15 Aldrin A 4294.2 4416.8 10.00 10.40 pg/uL 4 15 Heptachlor epoxide A 3663.1 3767.2 10.00 10.52 pg/uL 5 15 gamma-Chlordane A 3686.5 3642.3 10.00 10.30 pg/uL 3 15 alpha-Chlordane A 3470.5 3489.8 10.00 10.53 pg/uL 5 15 4,4'-DDE A 3241.8 3520.1 20.00 20.01 pg/uL 0 15 Endosulfan I A 3386.3 3506.5 10.00 10.87 pg/uL 9 15 Dieldrin A 3598.2 5315.7 20.00 24.45 pg/uL 22 15 c+ *** Endrin A 3003.2 3221. 6 20.00 18.87 pg/uL -6 15 4,4'-DDD A 2295. 6 1966.1 20.00 17.86 pg/uL -11 15 Endosulfan II A 3259.1 4037.1 20.00 22.72 pg/uL 14 15 4,4'-DDT A 2582. 9 2337.7 20.00 17.85 pg/uL -11 15 Endrin aldehyde A 2311.2 2468.7 20.00 21.54 pg/uL 8 15 Methoxychlor A 959.59 1331. 9 100.0 116.5 pg/uL 17 15 c+ *** Endosulfan sulfate A 2536. 6 2535.2 20.00 20.36 pg/uL 2 15 TCMX A 2695.3 2596.2 20.00 21.58 pg/uL 8 15 Decachlorobiphenyl A 1728.4 1678.1 20.00 20.80 pg/uL 4 15 alpha-BHC B 3776.3 4799.5 10.00 13.07 pg/uL 31 15 c+ *** gamma-BHC B 3139.7 4244. 9 10.00 13. 94 pg/uL 39 15 c+ *** beta-BHC B 1586.2 1968.8 10.00 12.37 pg/uL 24 15 c+ *** delta-BHC B 2207.3 3284. 9 10.00 15.49 pg/uL 55 15 c+ *** Heptachlor B 4382.7 4701.4 10.00 11.10 pg/uL 11 15 Aldrin B 3513.3 4271. 9 10.00 12.75 pg/uL 28 15 c+ *** Heptachlor epoxide B 3041.4 3729.7 10.00 12.78 pg/uL 28 15 c+ *** gamma-Chlordane B 2994.3 3629.3 10.00 12.12 pg/uL 21 15 c+ *** alpha-Chlordane B 2774.5 3423.4 10.00 12. 97 pg/uL 30 15 c+ *** 4,4'-DDE B 2183.4 3153.3 20.00 29. 62 pg/uL 48 15 c+ *** Endosulfan I B 2888.4 3528.1 10.00 12.81 pg/uL 28 15 c+ *** Dieldrin B 3431.8 3781.5 20.00 23.34 pg/uL 17 15 c+ *** Endrin B 1575.4 905.00 20.00 14.44 pg/uL -28 15 c- *** 4,4'-DDD B 1326.5 2558.2 20.00 36. 61 pg/uL 83 15 c+ *** Endosulfan II B 3292.5 3361.0 20.00 22. 69 pg/uL 13 15 4,4'-DDT B 1907.5 1977.2 20.00 23.16 pg/uL 16 15 c+ *** Endrin aldehyde B 2482.0 2524.1 20.00 22.26 pg/uL 11 15 Methoxychlor B 615. 91 925.88 100.0 150.7 pg/uL 51 15 c+ *** Endosulfan sulfate B 2188.2 2301.5 20.00 23.21 pg/uL 16 15 c+ *** TCMX B 1823. 9 2713.8 20.00 29.10 pg/uL 45 15 c+ Decachlorobiphenyl B 1819.4 2430.7 20.00 26.72 pg/uL 34 15 c+ Average EPA 8081A A (n=23) 8 15 Average EPA 8081A B (n=23) 31 15 ac *** TFB 02/05/10 : Corrected automatically drawn baseline. average ICAL %RSD out (A) Page 1 0' 2 240050803022 96 of 295