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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC23 Run Name : PEST 3 IDF : 1 . 0 Seqnum : 800049350007 File : 034 007 Time : 03-FEB-2010 17 : 57 Cal : 800046786001 Caldate : 01-FEB-2010 Standards : 513886 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 9990.8 14849 10.00 14.86 pg/uL 49 15 c+ *** gamma-BHC A 9273.0 13611 10.00 14. 68 pg/uL 47 15 c+ *** beta-BHC A 3724.4 5407. 9 10.00 14.52 pg/uL 45 15 c+ *** delta-BHC A 8286.7 11746 10.00 14.17 pg/uL 42 15 c+ *** Heptachlor A 8176.7 11282 10.00 13.80 pg/uL 38 15 c+ *** Aldrin A 8870.4 12982 10.00 14. 64 pg/uL 46 15 c+ *** Heptachlor epoxide A 7858.7 11395 10.00 14.50 pg/uL 45 15 c+ *** gamma-Chlordane A 7491.1 10876 10.00 14.52 pg/uL 45 15 c+ *** alpha-Chlordane A 7274.1 10468 10.00 14.39 pg/uL 44 15 c+ *** 4,4'-DDE A 6713. 6 9052.7 20.00 29.03 pg/uL 45 15 c+ *** Endosulfan I A 7116.0 10311 10.00 14.49 pg/uL 45 15 c+ *** Dieldrin A 8358.4 11405 20.00 26. 61 pg/uL 33 15 c+ *** Endrin A 6534.4 8315.5 20.00 26.23 pg/uL 31 15 c+ *** 4,4'-DDD A 4838.3 6661.1 20.00 31.42 pg/uL 57 15 c+ *** Endosulfan II A 7058. 9 9298. 6 20.00 26.35 pg/uL 32 15 c+ *** 4,4'-DDT A 4967.8 5252.8 20.00 24.33 pg/uL 22 15 c+ *** Endrin aldehyde A 4894.1 6578.8 20.00 26.88 pg/uL 34 15 c+ *** Methoxychlor A 2138.2 2361.5 100.0 134.1 pg/uL 34 15 c+ *** Endosulfan sulfate A 5317.3 7156.8 20.00 26. 92 pg/uL 35 15 c+ *** TCMX A 5922.4 8975. 6 20.00 30.31 pg/uL 52 15 c+ Decachlorobiphenyl A 6141.8 7351. 6 20.00 23. 94 pg/uL 20 15 c+ alpha-BHC B 26122 26579 10.00 10.27 pg/uL 3 15 gamma-BHC B 22257 23109 10.00 10.38 pg/uL 4 15 beta-BHC B 9682.2 10008 10.00 9. 913 pg/uL -1 15 delta-BHC B 21256 22729 10.00 11.01 pg/uL 10 15 Heptachlor B 20827 20017 10.00 8.771 pg/uL -12 15 Aldrin B 19867 22384 10.00 10.40 pg/uL 4 15 Heptachlor epoxide B 17417 19172 10.00 10.14 pg/uL 1 15 gamma-Chlordane B 18740 18667 10.00 10.26 pg/uL 3 15 alpha-Chlordane B 16903 17716 10.00 10.70 pg/uL 7 15 4,4'-DDE B 14080 16398 20.00 20. 97 pg/uL 5 15 Endosulfan I B 16409 17138 10.00 10. 67 pg/uL 7 15 Dieldrin B 14644 17582 20.00 21.89 pg/uL 9 15 Endrin B 11808 14409 20.00 22.28 pg/uL 11 15 4,4'-DDD B 11283 12504 20.00 20.14 pg/uL 1 15 Endosulfan II B 12588 14512 20.00 21.04 pg/uL 5 15 4,4'-DDT B 11389 11869 20.00 18.72 pg/uL -6 15 Endrin aldehyde B 9678.8 10940 20.00 20.86 pg/uL 4 15 Methoxychlor B 3749.7 4198. 9 100.0 101.2 pg/uL 1 15 Endosulfan sulfate B 9863. 9 11610 20.00 21. 65 pg/uL 8 15 TCMX B 13820 13777 20.00 19. 94 pg/uL 0 15 Decachlorobiphenyl B 7632.0 8740. 9 20.00 21.34 pg/uL 7 15 Average EPA 8081A A (n=23) 40 15 ac *** Average EPA 8081A B (n=23) 5 15 TFB 02/05/10 : Corrected automatically drawn baseline. average ICAL %RSD out (B) Page 1 0' 2 800049350007 98 of 295