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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC23 Run Name : PEST 4 IDF : 1 . 0 Seqnum : 800049350019 File : 034 019 Time : 04-FEB-2010 00 : 03 Cal : 800046786001 Caldate : 01-FEB-2010 Standards : 513887 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 9990.8 18172 20.00 36.38 pg/uL 82 15 c+ *** gamma-BHC A 9273.0 16387 20.00 35.34 pg/uL 77 15 c+ *** beta-BHC A 3724.4 5984.3 20.00 32.14 pg/uL 61 15 c+ *** delta-BHC A 8286.7 13996 20.00 33.78 pg/uL 69 15 c+ *** Heptachlor A 8176.7 13259 20.00 32.43 pg/uL 62 15 c+ *** Aldrin A 8870.4 15970 20.00 36.01 pg/uL 80 15 c+ *** Heptachlor epoxide A 7858.7 13561 20.00 34.51 pg/uL 73 15 c+ *** gamma-Chlordane A 7491.1 12992 20.00 34. 69 pg/uL 73 15 c+ *** alpha-Chlordane A 7274.1 12486 20.00 34.33 pg/uL 72 15 c+ *** 4,4'-DDE A 6713. 6 11286 40.00 65.33 pg/uL 63 15 c+ *** Endosulfan I A 7116.0 12301 20.00 34.57 pg/uL 73 15 c+ *** Dieldrin A 8358.4 16450 40.00 69.48 pg/uL 74 15 c+ *** Endrin A 6534.4 11048 40.00 59.73 pg/uL 49 15 c+ *** 4,4'-DDD A 4838.3 8279.5 40.00 67.77 pg/uL 69 15 c+ *** Endosulfan II A 7058. 9 12243 40.00 69.37 pg/uL 73 15 c+ *** 4,4'-DDT A 4967.8 6463.5 40.00 52.03 pg/uL 30 15 c+ *** Endrin aldehyde A 4894.1 7968.8 40.00 65.13 pg/uL 63 15 c+ *** Methoxychlor A 2138.2 3054. 6 200.0 272. 9 pg/uL 36 15 c+ *** Endosulfan sulfate A 5317.3 8743.5 40.00 65.77 pg/uL 64 15 c+ *** TCMX A 5922.4 10552 40.00 71.27 pg/uL 78 15 c+ Decachlorobiphenyl A 6141.8 8168.7 40.00 53.20 pg/uL 33 15 c+ alpha-BHC B 26122 25267 20.00 21.21 pg/uL 6 15 gamma-BHC B 22257 21404 20.00 19.23 pg/uL -4 15 beta-BHC B 9682.2 9297.2 20.00 20.36 pg/uL 2 15 delta-BHC B 21256 20323 20.00 20. 97 pg/uL 5 15 Heptachlor B 20827 21236 20.00 19.73 pg/uL -1 15 Aldrin B 19867 20467 20.00 20.22 pg/uL 1 15 Heptachlor epoxide B 17417 17600 20.00 19. 94 pg/uL 0 15 gamma-Chlordane B 18740 17079 20.00 20.89 pg/uL 4 15 alpha-Chlordane B 16903 16168 20.00 21.27 pg/uL 6 15 4,4'-DDE B 14080 14385 40.00 39. 63 pg/uL -1 15 Endosulfan I B 16409 15491 20.00 20. 99 pg/uL 5 15 Dieldrin B 14644 14938 40.00 42. 91 pg/uL 7 15 Endrin B 11808 12589 40.00 43. 60 pg/uL 9 15 4,4'-DDD B 11283 12155 40.00 41.59 pg/uL 4 15 Endosulfan II B 12588 12746 40.00 41.49 pg/uL 4 15 4,4'-DDT B 11389 10730 40.00 36.23 pg/uL -9 15 Endrin aldehyde B 9678.8 9641.2 40.00 39.56 pg/uL -1 15 Methoxychlor B 3749.7 3459.8 200.0 203.8 pg/uL 2 15 Endosulfan sulfate B 9863. 9 10240 40.00 41. 69 pg/uL 4 15 TCMX B 13820 13753 40.00 39.81 pg/uL 0 15 Decachlorobiphenyl B 7632.0 7224.7 40.00 37.01 pg/uL -7 15 Average EPA 8081A A (n=23) 65 15 ac *** Average EPA 8081A B (n=23) 4 15 TFB 02/05/10 : Corrected automatically drawn baseline. average ICAL %RSD out (B) Page 1 0' 2 800049350019 100 of 295