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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC23 Run Name : PEST_4 IDF : 1 . 0 Seqnum : 800052495004 File : 036 004 Time : 05-FEB-2010 12 : 04 Cal : 800046786001 Caldate : 01-FEB-2010 Standards : 513887 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 9990.8 16911 20.00 33.85 pg/uL 69 15 c+ *** gamma-BHC A 9273.0 15179 20.00 32.74 pg/uL 64 15 c+ *** beta-BHC A 3724.4 5582.5 20.00 29. 98 pg/uL 50 15 c+ *** delta-BHC A 8286.7 13451 20.00 32.46 pg/uL 62 15 c+ *** Heptachlor A 8176.7 12245 20.00 29. 95 pg/uL 50 15 c+ *** Aldrin A 8870.4 14508 20.00 32.71 pg/uL 64 15 c+ *** Heptachlor epoxide A 7858.7 12372 20.00 31.49 pg/uL 57 15 c+ *** gamma-Chlordane A 7491.1 11892 20.00 31.75 pg/uL 59 15 c+ *** alpha-Chlordane A 7274.1 11375 20.00 31.28 pg/uL 56 15 c+ *** 4,4'-DDE A 6713. 6 10642 40.00 62.07 pg/uL 55 15 c+ *** Endosulfan I A 7116.0 11111 20.00 31.23 pg/uL 56 15 c+ *** Dieldrin A 8358.4 14378 40.00 61.02 pg/uL 53 15 c+ *** Endrin A 6534.4 10072 40.00 54. 99 pg/uL 37 15 c+ *** 4,4'-DDD A 4838.3 7840.7 40.00 64.86 pg/uL 62 15 c+ *** Endosulfan II A 7058. 9 11083 40.00 62.80 pg/uL 57 15 c+ *** 4,4'-DDT A 4967.8 6203. 9 40.00 50.29 pg/uL 26 15 c+ *** Endrin aldehyde A 4894.1 7370.5 40.00 60.24 pg/uL 51 15 c+ *** Methoxychlor A 2138.2 3098. 6 200.0 275. 6 pg/uL 38 15 c+ *** Endosulfan sulfate A 5317.3 8237.8 40.00 61. 97 pg/uL 55 15 c+ *** TCMX A 5922.4 9768. 6 40.00 65. 98 pg/uL 65 15 c+ Decachlorobiphenyl A 6141.8 7783.3 40.00 50. 69 pg/uL 27 15 c+ alpha-BHC B 26122 24710 20.00 20.70 pg/uL 4 15 gamma-BHC B 22257 21287 20.00 19.13 pg/uL -4 15 beta-BHC B 9682.2 9123.8 20.00 19. 94 pg/uL 0 15 delta-BHC B 21256 20076 20.00 20. 69 pg/uL 3 15 Heptachlor B 20827 20279 20.00 18.75 pg/uL -6 15 Aldrin B 19867 20442 20.00 20.19 pg/uL 1 15 Heptachlor epoxide B 17417 17700 20.00 20.07 pg/uL 0 15 gamma-Chlordane B 18740 17557 20.00 21.54 pg/uL 8 15 alpha-Chlordane B 16903 16451 20.00 21. 68 pg/uL 8 15 4,4'-DDE B 14080 14886 40.00 41.25 pg/uL 3 15 Endosulfan I B 16409 16070 20.00 21.86 pg/uL 9 15 Dieldrin B 14644 15296 40.00 44.24 pg/uL 11 15 Endrin B 11808 12807 40.00 44.53 pg/uL 11 15 4,4'-DDD B 11283 12412 40.00 42.58 pg/uL 6 15 Endosulfan II B 12588 13191 40.00 43.28 pg/uL 8 15 4,4'-DDT B 11389 11070 40.00 37.54 pg/uL -6 15 Endrin aldehyde B 9678.8 10193 40.00 42.20 pg/uL 6 15 Methoxychlor B 3749.7 3466.3 200.0 204.3 pg/uL 2 15 Endosulfan sulfate B 9863. 9 10608 40.00 43.46 pg/uL 9 15 TCMX B 13820 12970 40.00 37.54 pg/uL -6 15 Decachlorobiphenyl B 7632.0 7838.3 40.00 40.56 pg/uL 1 15 Average EPA 8081A A (n=23) 53 15 ac *** Average EPA 8081A B (n=23) 6 15 TFB 02/05/10 : Corrected automatically drawn baseline. average ICAL %RSD out (B) Page 1 0' 2 800052495004 102 of 295