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CURTIS & TOMPKINS CONTINUING CALIBRATION FOR 218019 PEST Soil EPA 8081A Inst : GC23 Run Name : PEST_3 IDF : 1 . 0 Seqnum : 800052495007 File : 036 007 Time : 05-FEB-2010 17 : 01 Cal : 800046786001 Caldate : 01-FEB-2010 Standards : 513886 Avg Analyte Ch RF/CF RF/CF Spiked Quant Units %D Max %D Flags alpha-BHC A 9990.8 15167 10.00 15.18 pg/uL 52 15 c+ *** gamma-BHC A 9273.0 13513 10.00 14.57 pg/uL 46 15 c+ *** beta-BHC A 3724.4 5359.4 10.00 14.39 pg/uL 44 15 c+ *** delta-BHC A 8286.7 12265 10.00 14.80 pg/uL 48 15 c+ *** Heptachlor A 8176.7 11150 10.00 13. 64 pg/uL 36 15 c+ *** Aldrin A 8870.4 13106 10.00 14.77 pg/uL 48 15 c+ *** Heptachlor epoxide A 7858.7 11534 10.00 14. 68 pg/uL 47 15 c+ *** gamma-Chlordane A 7491.1 11011 10.00 14.70 pg/uL 47 15 c+ *** alpha-Chlordane A 7274.1 10663 10.00 14. 66 pg/uL 47 15 c+ *** 4,4'-DDE A 6713. 6 9500.1 20.00 30.31 pg/uL 52 15 c+ *** Endosulfan I A 7116.0 10457 10.00 14. 69 pg/uL 47 15 c+ *** Dieldrin A 8358.4 11168 20.00 26.15 pg/uL 31 15 c+ *** Endrin A 6534.4 8408. 6 20.00 26.46 pg/uL 32 15 c+ *** 4,4'-DDD A 4838.3 7152.0 20.00 33.44 pg/uL 67 15 c+ *** Endosulfan II A 7058. 9 9531.1 20.00 27.00 pg/uL 35 15 c+ *** 4,4'-DDT A 4967.8 5257. 9 20.00 24.35 pg/uL 22 15 c+ *** Endrin aldehyde A 4894.1 6745.0 20.00 27.56 pg/uL 38 15 c+ *** Methoxychlor A 2138.2 2374.3 100.0 134.7 pg/uL 35 15 c+ *** Endosulfan sulfate A 5317.3 7364.0 20.00 27.70 pg/uL 38 15 c+ *** TCMX A 5922.4 9028.2 20.00 30.49 pg/uL 52 15 c+ Decachlorobiphenyl A 6141.8 7062. 6 20.00 23.00 pg/uL 15 15 alpha-BHC B 26122 27355 10.00 10. 63 pg/uL 6 15 gamma-BHC B 22257 24068 10.00 10.81 pg/uL 8 15 beta-BHC B 9682.2 9864.8 10.00 9.739 pg/uL -3 15 delta-BHC B 21256 23061 10.00 11.19 pg/uL 12 15 Heptachlor B 20827 23906 10.00 10.59 pg/uL 6 15 Aldrin B 19867 23088 10.00 10.75 pg/uL 8 15 Heptachlor epoxide B 17417 20136 10.00 10.70 pg/uL 7 15 gamma-Chlordane B 18740 20107 10.00 11.25 pg/uL 12 15 alpha-Chlordane B 16903 18689 10.00 11.40 pg/uL 14 15 4,4'-DDE B 14080 17124 20.00 22.00 pg/uL 10 15 Endosulfan I B 16409 18245 10.00 11.49 pg/uL 15 15 Dieldrin B 14644 18426 20.00 23.24 pg/uL 16 15 c+ *** Endrin B 11808 15408 20.00 24.14 pg/uL 21 15 c+ *** 4,4'-DDD B 11283 14012 20.00 22.74 pg/uL 14 15 Endosulfan II B 12588 15291 20.00 22.41 pg/uL 12 15 4,4'-DDT B 11389 13192 20.00 21.03 pg/uL 5 15 Endrin aldehyde B 9678.8 11597 20.00 22.26 pg/uL 11 15 Methoxychlor B 3749.7 4857.4 100.0 124.7 pg/uL 25 15 c+ *** Endosulfan sulfate B 9863. 9 12497 20.00 23.55 pg/uL 18 15 c+ *** TCMX B 13820 14728 20.00 21.31 pg/uL 7 15 Decachlorobiphenyl B 7632.0 9296.5 20.00 22.81 pg/uL 14 15 Average EPA 8081A A (n=23) 42 15 ac *** Average EPA 8081A B (n=23) 12 15 TFB 02/05/10 : Corrected automatically drawn baseline. average ICAL %RSD out (B) Page 1 0' 2 800052495007 104 of 295