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CURTIS & TOMPKINS SEQUENCE SUMMARY FOR 800049350 Instrument : GC23 Begun : 02/03/10 06 : 30 Method : EPA 8081A SOP Version : pesticides rvl2 # File Type Sample ID Matrix Batch Analyzed IDF Stds Used 001 034 001 X PRIMER 02/03/10 06:30 1.0 002 034 002 X HEX 02/03/10 06:53 1.0 003 034_003 X HEX 02/03/10 07:15 1.0 004 034_004 PEM PEM 02/03/10 07:37 1.0 1 005 034 005 X CCV 02/03/10 07:59 1.0 2 006 034_006 X HEX 02/03/10 17:35 1.0 007 034_007 CCV PEST_3 02/03/10 17:57 1.0 2 008 =34_00fjX IQC531257 oil 1159701[02/03/10 19:59 1.0 009 034_009 BS QC531258 Soil 159701 02/03/10 20:21 1.0 010 034_010 BSD QC531259 Soil 159701 02/03/10 20:43 1.0 011 034 011 SAMPLE 218019-001 Soil 159701 02/03/10 21:05 1.0 012 034 012 SAMPLE 217976-012 Soil 159701 02/03/10 21:27 20.0 013 034 013 SAMPLE 217976-012 Soil 159701 02/03/10 21:50 20.0 014 034 014 MSS 218117-001 Soil 159737 02/03/10 22:12 1.0 3:ENDOSULFANS=690 015 034 015 SAMPLE 218117-002 Soil 159737 02/03/10 22:34 3.0 3:ACHLORDANE=530 016 034 016 SAMPLE 218117-003 Soil 159737 02/03/10 22:56 1.0 1:ISODRIN=130 017 034_017 SAMPLE 218117-004 Soil 159737 02/03/10 23:18 3.0 2:ALDRIN=350 018 034_018 PEM PEM 02/03/10 23:40 1.0 1 019 034_019 CCV PEST-4 02/04/10 00:03 1.0 3 020 034 020 X CCV 02/04/10 00:25 1.0 3 021 034 021 X PEM 02/04/10 00:47 1.0 1 022 034 022 BLANK QC531403 Soil 159737 02/04/10 01:09 1.0 023 034 023 LCS QC531404 Soil 159737 02/04/10 01:31 1.0 024 034 024 X QC531405 Soil 159737 02/04/10 01:53 1.0 5:ENDOSULFANS=680 025 034 025 X QC531406 Soil 159737 02/04/10 02:15 1.0 4:BHCALPHA=210 026 034 026 PEM PEM 02/04/10 02:38 1.0 1 027 034 027 CCV PEST3 02/04/10 03:00 1.0 2 028 034 028 CCV PEST 3 02/04/10 03:22 1.0 2 029 034 029 X PEM 02/04/10 03:44 1.0 1 030 034 030 X HEX 02/04/10 04:06 1.0 TFB 02/04/10 : I verified that the vials loaded on the instrument matched the sequence data entry, for runs 1 through 30 . Standards used: 1=S13336 2=S13886 3=S13887 Page 1 of 1 109 of 295