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CURTIS & TOMPKINS INITIAL CALIBRATION FOR 218019 PCBS Soil : EPA 8082 <br /> Inst : GC06 Name : 1660_026 <br /> Calnum : 200038197001 Date : 26-JAN-2010 21 : 52 <br /> Units : pg/uL X Axis : R <br /> Level File Seqnum Sample ID Analyzed Stds <br /> Ll 026_019 200038197019 PCB10 2 26-JAN-2010 21:52 512698 <br /> L2 026_020 200038197020 PCB25 5 26-JAN-2010 22:19 512700 <br /> L3 026_021 200038197021 PCB100 20 26-JAN-2010 22:47 512701 <br /> L4 026_022 200038197022 PCB250 50 26-JAN-2010 23:14 513489 <br /> L5 026_023 200038197023 PCB500 100 26-JAN-2010 23:42 513600 <br /> L6 026_024 200038197024 PCB750 150 27-JAN-2010 00:10 512704 <br /> L7 026_025 200038197025 PCB1000 200 27-JAN-2010 00:37 512705 <br /> r^2 <br /> Analyte h Ll L2 L3 L4 L5 L6 L7 Type a0 al Avg %RSD MnR^2 MxRSD Flg <br /> Aroclor-1016 Peak # 1 A 386.30 374.64 335.36 324.06 293.20 276.44 252.15 AVRG 0.00312 320.31 16 .99 20 <br /> Aroclor-1016 Peak # 2 A 341.80 319.56 321.34 327.90 334.24 337.23 308.55 AVRG 0.00306 327.23 4 .99 20 <br /> Aroclor-1016 Peak # 3 A 210.00 203.92 199.23 217.83 207.23 200.09 184.26 AVRG 0.00492 203.22 5 .99 20 <br /> Aroclor-1016 Peak # 4 A 126.20 134.44 113.87 126.69 113.24 112.67 96.756 AVRG 0.00850 117.70 11 .99 20 <br /> Aroclor-1016 Peak # 5 A 217.60 212.48 194.26 202.93 196.40 182.44 173.20 AVRG 0.00507 197.04 8 .99 20 <br /> Aroclor-1260 Peak # 1 A 657.40 630.44 528.95 531.66 519.77 496.68 449.63 AVRG 0.00184 544.93 13 .99 20 <br /> Aroclor-1260 Peak # 2 A 370.30 365.68 315.40 318.19 314.35 303.10 271.10 AVRG 0.00310 322.59 11 .99 20 <br /> Aroclor-1260 Peak # 3 A 376.90 367.52 320.80 333.58 338.43 334.09 296.49 AVRG 0.00296 338.26 8 .99 20 <br /> Aroclor-1260 Peak # 4 A 749.70 713.44 620.78 650.68 684.65 677.47 607.28 AVRG 0.00149 672.00 7 .99 20 <br /> Aroclor-1260 Peak # 5 A 348.60 342.08 306.94 331.02 360.83 363.56 327.47 AVRG 0.00294 340.07 6 .99 20 <br /> TCMX A 6074.0 6069.2 5349.2 6751.6 6625.8 6435.2 5647.6 AVRG 1.63E-4 6136.1 8 .99 20 <br /> Decachlorobiphenyl A 8342.5 7723.6 6828.0 6722.7 6895.1 6663.4 5756.8 AVRG 1.43E-4 6990.3 12 .99 20 <br /> Aroclor-1016 Peak # 1 B 96.300 112.56 99.990 112.15 102.90 98.252 89.159 AVRG 0.00984 101.62 8 .99 20 <br /> Aroclor-1016 Peak # 2 B 117.00 111.28 108.29 121.40 116.99 115.61 106.37 AVRG 0.00878 113.85 5 .99 20 <br /> Aroclor-1016 Peak # 3 B 248.10 286.48 281.29 321.95 326.73 329.65 306.19 AVRG 0.00333 300.06 10 .99 20 <br /> Aroclor-1016 Peak # 4 B 152.30 142.08 137.75 152.26 149.71 148.75 136.84 AVRG 0.00686 145.67 5 .99 20 <br /> Aroclor-1016 Peak # 5 B 91.600 80.480 79.870 87.592 83.152 82.741 75.371 AVRG 0.01205 82.972 6 .99 20 <br /> Aroclor-1260 Peak # 1 B 356.20 278.88 272.99 299.86 321.29 319.82 294.84 AVRG 0.00327 306.27 9 .99 20 <br /> Aroclor-1260 Peak # 2 B 288.80 277.24 255.28 275.72 285.33 280.56 253.67 AVRG 0.00365 273.80 5 .99 20 <br /> Aroclor-1260 Peak # 3 B 220.80 214.32 196.51 213.06 225.13 225.61 204.46 AVRG 0.00467 214.27 5 .99 20 <br /> Aroclor-1260 Peak # 4 B 566.50 519.92 508.41 552.62 635.40 636.23 574.39 AVRG 0.00175 570.49 9 .99 20 <br /> Aroclor-1260 Peak # 5 B 260.30 248.24 228.67 256.32 290.16 296.05 270.37 AVRG 0.00378 264.30 9 .99 20 <br /> TCMX B 3481.5 3324.8 3253.8 3949.5 4039.5 4077.8 3828.5 AVRG 2.70E-4 3707.9 9 .99 20 <br /> Decachlorobiphenyl j B 6320.0 6015.6 5852.3 6082.1 6317.9 6138.1 5281.3 AVRG I 1.67E-4 6001.0 6 1 .99 20 <br /> Page 1 of 2 200038197001 <br /> 122 of 295 <br />