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CURTIS & TOMPKINS SEQUENCE SUMMARY FOR 200052491 Instrument : GC06 Begun : 02/05/10 10 : 51 Method : EPA 8082 SOP Version : pcb rv. 7 # I File I Type ISample ID Matrix Batch Analyzed I IDF Stds Used 001 1036_001 X IHEX 02/05/10 10:51 1.0 002 036_002 CCV PCB250_50 02/05/10 11:18 1.0 003 1036 003 CCV AR2154 02/05/10 12:0711.0 2 004 036 004 X SPIKETEST 02/05/10 12:35 1.0 005 036 005 LCS QC530935 Soil 159621 02/05/10 13:02 1.0 006 036 006 LCS QC531057 Soil 159653 02/05/10 13:30 1.0 007 036 007 SAMPLE 217954-017 Soil 159621 02/05/10 13:58 5.0 008 036_008 MSS 217954-018 Soil 159621 02/05/10 14:25 2.0 009 036_009 MS QC530936 Soil 159621 02/05/10 15:11 2.0 010 036_010 MSD QC530937 Soil 159621 02/05/10 15:39 2.0 011 036 011 SAMPLE 217954-009 Soil 159583 02/05/10 16:06 1.0 012 036 012 SAMPLE 217954-013 Soil 159583 02/05/10 16:34 1.0 013 036 013 SAMPLE 217954-014 Soil 159583 02/05/10 17:02 1.0 014 036 014 SAMPLE 217954-017 Soil 159621 02/05/10 17:29 10.0 015 036_015 CCV PCB500_100 02/05/10 17:57 1.0 3 016 036 016 CCV AR2154 02/05/10 18:25 1.0 2 017 036 017 CCV AR1248 02/05/10 19:00 1.0 4 018 036 018 SAMPLE 218033-001 Miscell. 159653 02/05/10 19:28 100.0 5:PCB1260#1=5900 019 036 019 SAMPLE 218043-001 Miscell. 159653 02/05/10 19:55 1.0 020 036 020 BLANK QC530683 Soil 159549 02/05/10 20:23 1.0 021 036 021 LCS QC530684 Soil 159549 02/05/10 20:50 1.0 022 036 022 SAMPLE 217969-023 Soil 159549 02/05/10 21:18 1.0 4:PCB1016#5=5700 023 036 023 SAMPLE 217969-024 Soil 159549 02/05/10 21:46 1.0 4:PCB1016#5=3000 024 036 024 SAMPLE 217969-025 Soil 159549 02/05/10 22:13 1.0 025 036 025 SAMPLE 217969-026 Soil 159549 02/05/10 22:41 1.0 1:PCB1248#5=1500 026 036 026 MSS 217969-028 Soil 159549 02/05/10 23:08 1.0 4:PCB1016#5=4900 027 036 027 SAMPLE 217969-029 Soil 159549 02/05/10 23:36 1.0 028 036 028 CCV PCB250 50 02/06/10 00:04 1.0 1 029 036 029 X CCV 02/06/10 00:31 1.0 1 030 036 030 CCV AR2154 02/06/10 00:59 1.0 2 031 036 031 CCV AR1248 02/06/10 01:26 1.0 4 032 036 032 SAMPLE 217994-001 Miscell. 159549 02/06/10 01:54 1.0 033 036 033 SAMPLE 217994-002 Miscell. 159549 02/06/10 02:21 1.0 034 036 034 SAMPLE 217994-003 Miscell. 159549 02/06/10 02:49 1.0 035 036 035 SAMPLE 217994-004 Miscell. 159549 02/06/10 03:17 1.0 036 036 036 SAMPLE 217994-005 Miscell. 159549 02/06/10 03:44 1.0 037 036 037 MSS 217994-006 Miscell. 159549 02/06/10 04:12 1.0 038 036 038 SAMPLE 217994-007 Miscell. 159549 02/06/10 04:39 1.0 039 036 039 SAMPLE 217994-008 Miscell. 159549 02/06/10 05:07 1.0 040 036 040 SAMPLE 217994-009 Miscell. 159549 02/06/10 05:34 1.0 041 036 041 SAMPLE 217994-010 Miscell. 159549 02/06/10 06:02 1.0 042 036 042 CCV PCB500 100 02/06/10 06:30 1.0 3 043 036 043 X CCV 02/06/10 06:57 1.0 3 044 036 044 CCV AR2154 02/06/10 07:25 1.0 2 045 036 045 CCV AR1248 02/06/10 07:52 1.0 4 046 036 046 SAMPLE 217994-011 Miscell. 159549 02/06/10 08:20 1.0 3:PCB1016#1=3800 047 036 047 SAMPLE 217994-012 Miscell. 159549 02/06/10 08:47 1.0 048 036 048 SAMPLE 217994-013 Miscell. 159549 02/06/10 09:15 1.0 049 036 049 MS QC530685 Soil 159549 02/06/10 09:42 1.0 3:PCB1016#5=3700 050 036 050 MSD QC530686 Soil 159549 02/06/10 10:10 1.0 3:PCB1016#5=3600 051 036 051 MS QC530687 Miscell. 159549 02/06/10 10:37 1.0 052 036 052 MSD QC530688 Miscell. 159549 02/06/10 11:05 1.0 Page 1 of 2 138 of 295