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CURTIS & TOMPKINS SEQUENCE SUMMARY FOR 90052309 Instrument : MET09 Begun : 02/05/10 07 : 49 Method : EPA 6010B SOP Version : icp metals =9 # File Type Sample ID Matrix Batch I Analyzed I TDF I Std., Used 053 met09 sn 6010a SAMPLE 218133-005 Filtrate 159788 02/05/10 13:09 1.0 1 3:NA=120000 054 met09 sn 6010a X 02/05/10 13:16 1.0 9 055 met09 sn 6010a CCV 02/05/10 13:28 1.0 9 056 met09 sn 6010a CCB 02/05/10 13:33 M1.0 057 met09 sn 6010a SAMPLE 218133-006 Filtrate 159788 02/05/10 13:38 1.0 3:CA=350000 058 met09 sn 6010a SAMPLE 218133-007 Filtrate 159788 02/05/10 13:44 1.0 059 met09 sn 6010a SAMPLE 218133-008 Filtrate 159788 02/05/10 13:49 1.0 060 met09 sn 6010a SAMPLE 218133-009 Filtrate 159788 02/05/10 13:54 1.0 3:MG=230000 061 met09 sn 6010a SAMPLE 218133-010 Filtrate 159788 02/05/10 14:02 1.0 3:MG=240000 062 met09 sn 6010a SAMPLE 218133-011 Filtrate 159788 02/05/10 14:09 1.0 063 met09_sn_6010a TCSAB 02/05/10 14:14 1.0 8 5:CA=450000 064 met09_sn_6010a RINSE 02/05/10 14:20 1.0 065 met09 sn 6010a BLANK QC531614 Soil 159791 02/05/10 14:25 1.0 066 met09_sn_6010a BS QC331613 Soil 159791 02/05/10 14:30 1.0 067 met09 sn 6010a IX 02/05/10 14:34 1.0 9 068 met09 sn 6010a CCV 02/05/10 14:39 1.0 9 069 met09 sn 6010a CCB 02/05/10 14:44 1.0 070 met09 sn 6010a BSD QC331616 Soil 159791 02/05/10 14:49 1.0 071 met09 sn 6010a MSS 218019-001 Soil 159791 02/05/10 14:53 1.0 4:FE=300000 072 met09 sn 6010a MS QC331617 Soil 159791 02/05/10 14:56 1.0 4:FE=300000 073 met09 sn 6010a MSD QC331618 Soil 159791 02/05/10 15:01 1.0 4:FE=310000 074 met09 sn 6010a SER QC531619 Soil 159791 02/05/10 15:07 5.0 075 met09 sn 6010a PDS QC531620 Soil 159791 02/05/10 15:11 1.0 12 13 4:FE=290000 076 met09 sn 6010a SAMPLE 218162-004 Soil 159791 02/05/10 15:17 1.0 3:FE=330000 077 met09 sn 6010a SAMPLE 218162-006 Soil 159791 02/05/10 15:21 1.0 3:FE=370000 078 met09 sn 6010a TCSAB 02/05/10 15:25 1.0 8 S:MG=470000 079 met09 sn 6010a X RINSE 02/05/10 15:31 1.0 080 met09 sn 6010a X 02/05/10 15.36 1.0 9 081 met09 sn 6010a CCV 02/05/10 15:38 1.0 9 082 met09 sn 6010a CCB 02/05/10 15:43 1.0 083 met09 sn 6010a MSS 218019-001 Soil 159791 02/05/10 15:48 1.0 4:FE=340000 084 met09 sn 6010a BLANK QC531607 Water 159790 02/05/10 15:54 1.0 085 met09 sn 6010a BS QC531608 Water 159790 02/05/10 15:59 1.0 086 met09 sn 6010a BSD QC531609 Water 159790 02/05/10 16:03 1.0 087 met09 sn 6010a MSS 218139-013 Water 159790 02/05/10 16:08 1.0 2:MG=210000 088 met09 sn 6010a MS QC531610 Water 159790 02/05/10 16:15 1.0 089 met09 sn 6010a MSD QC531611 Water 159790 02/05/10 16:22 1.0 090 met09 sn 6010a SER QC531612 Water 159790 02/05/10 16:28 5.0 091 met09 sn 6010a PDS QC531613 Water 159790 02/05/10 16:35 1.0 10 11 1:MG=260000 092 met09 sn 6010a SAMPLE 218139-010 Water 159790 02/05/10 16:42 1.0 2:NA=340000 093 met09 sn 6010a CCV 02/05/10 16:49 1.0 9 094 met09 sn 6010a X 02/05/10 16:55 1.0 095 met09 sn 6010a CCB 02/05/10 16:58 1.0 096 met09 sn 6010a SAMPLE 218139-015 Water 159790 02/05/10 17:03 1.0 2:MG=210000 097 met09 sn 6010a SAMPLE 218133-001 Water 159790 02/05/10 17:11 1.0 098 met09 sn 6010a SAMPLE 218133-004 Water 159790 02/05/10 17:16 1.0 1:CA=110000 099 met09 sn 6010a SAMPLE 218133-005 Water 159790 02/05/10 17:21 1.0 3:NA=140000 100 met09 sn 6010a SAMPLE 218133-006 Water 159790 02/05/10 17:29 1.0 3:CA=320000 101 met09 sn 6010a SAMPLE 218133-007 Water 159790 02/05/10 17:36 1.0 102 met09 sn 6010a SAMPLE 218133-008 Water 159790 02/05/10 17:41 1.0 1:NA=110000 103 met09 sn 6010a SAMPLE 218133-009 Water 159790 02/05/10 17:49 1.0 3:MG=260000 104 met09 sn 6010a SAMPLE 218133-010 Water 159790 02/05/10 17:56 1.0 3:MG=270000 Page 2 of 3 163 of 295