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CURTIS & TOMPKINS INITIAL CALIBRATION FOR 218019 METALS Soil : EPA 6010B Inst : MET09 Reviewer --- Calnum : 90052309001 Date : 05-FEB-2010 07 : 49 Units : ug/L X Axis : R Level File Seqnum Sample TD Analyzed Stds L1 met09 sn 6010a 90052309002 CRT5.1 05-FEB-2010 07:54 S13742 L2 met09 sn 6010a 90052309003 CS100 05-FEB-2010 08:00 S13802 L3 met09 sn 6010a 90052309004 CS1K 05-FEB-2010 08:04 S13801 L4 met09 sn 6010a 90052309005 CS10K 05-FEB-2010 08:08 S13743 L5 met09 sn 6010a 90052309006 CS100K 05-FEB-2010 08:14 S13418 r^2 Analyte Ch Ll L2 L3 L4 L5 Type a0al a2 Avg %RSD MnR^2 F Antimony A 9.8200 10.737 11.012 11.113 LORD 0.00000 0.08999 10.670 1.000 0.995 Arsenic A 5.3000 5.6840 5.8660 5.5871 LORD 0.00000 0.17890 5.6093 1.000 0.995 Barium A 68.860 65.898 67.433 67.314 LORD 0.00000 0.01486 67.376 1.000 0.995 Beryllium A 3386.9 3534.7 3580.2 LORD 0.00000 2.79E-4 3500.6 1.000 0.995 Cadmium A 98.780 92.791 95.780 94.601 LORD 0.00000 0.01057 95.488 1.000 0.995 Chromium A 123.18 142.91 144.99 147.92 LORD 0.00000 0.00676 139.75 1.000 0.995 Cobalt A 42.040 42.406 44.604 44.268 LORD 0.00000 0.02259 43.330 1.000 0.995 Copper A 148.26 170.96 175.94 180.78 LORD 0.00000 0.00553 168.99 1.000 0.995 Lead A 28.680 30.515 31.209 31.302 LORD 0.00000 0.03195 30.427 1.000 0.995 Molybdenum A 24.680 22.871 22.971 23.003 LORD 0.00000 0.04347 23.381 1.000 0.995 Nickel A 57.220 63.718 68.210 68.243 LORD 0.00000 0.01465 64.348 1.000 0.995 Selenium A 7.5800 8.0500 8.3045 8.4812 LORD 0.00000 0.11793 8.1039 1.000 0.995 Silver A 323.56 313.01 319.46 321.56 LORD 0.00000 0.00311 319.40 1.000 0.995 Thallium A 5.2200 5.8750 6.1359 6.1011 LORD 0.00000 0.16390 5.8330 1.000 0.995 Vanadium A 152.48 166.95 169.09 173.59 LORD 0.00000 0.00576 165.53 1.000 0.995 Zinc A 46.215 43.328 44.075 44.188 LORO 0.00000 0.02263 44.451 1.000 0.995 Page 1 of 2 90052309001 167 of 295