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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 124-McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hhtW://www.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID:Union Safe Deposit Date Sampled: 09/23/98 <br /> 4005 North Wilson Way Bank;Soda Comers Date Received:09/24/98 <br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted: 09/28-09/29/98 <br /> Client P.O: Date Analyzed: 09/28-09/29/98 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 95711 <br /> Reporting Limit <br /> Client ID SPI <br /> Matrix W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(DIPS) ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND 5.0 1.0 <br /> tert-Butanol 8.1 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 98 <br /> Comments: i <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/,xipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />