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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htW://www.mccampbell.com E-mail:main@mccampbell.com <br /> Client Project ID:Union Safe Date Sampled:09/23/98 De <br /> Advanced GeoEnvirottmental J P <br /> 4005 North Wilson Way Bank;Soda Corners Date Received:09/24/98 <br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted: 10/09/98 <br /> Client P.O: Date Analyzed: 10/09/98 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 95712 <br /> Reporting Limit <br /> Client ID SP2 <br /> Matrix W S W <br /> Compound Concentration' ug/kg ug/L <br /> Di-isopropyl Ether(DIPE) ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETRE) ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND 5.0 1.0 <br /> tert-Butanol ND 25 5.0 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 <br /> Comments: <br /> •water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.%sediment;0)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />