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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccam bell corn E-mail main@mccampbell corn <br /> ' Date Sampled 08/28/99 <br /> Advanced GeoEnvironmental Client Project ID Brokides Petroleum <br />' 4005 North Wilson Way Date Received 08/31/99 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 08/31-09/07/99 <br /> __T' Client P O Date Analyzed 08131-09/07/99 <br /> Gasoline Range(C6-C12)Volatile Hydrocarbons as Gasoline*,with Methyl tert-Butyl Ether* & BTEX* <br /> EPA methods 5030 modified 8015,and 8020 or 602 California RW CB(SF BayRegion)method GCFID 5030 <br /> Ethylben- %Recovery <br /> Lab]D Client ID Matrix TPH(g) MTBE Benzene Toluene Zene Xylenes Surrogate <br />' 18247 BMW 1 W 5900a 85 340 200 260 1200 104 <br /> 18248 BMW 2 W 400,a 330 3 2 1 62 1 9 2 8 --- <br /> 18249 <br /> -"18249 BMW 3 W 250j ND 1 5 ND 4 1 2 9 119 <br /> 18250 BMW 4 W 36,000,a ND<200 1000 650 1400 8200 107 <br />' 18251 BMW 5 W 100,b ND ND ND ND 63 103 <br /> 18252 MW 5 W 3000,a 360 49 19 190 490 100 <br />' Reporting Limit unless W 50 uglL 5 0 0 5 0 5 0 5 0 5 <br /> othemise stated,ND <br /> means not detected above S 1 0 mg/kg 005 0 005 0 005 0 005 0 005 <br /> the reporting limit <br />' water and vapor samples are reported in ug/L,uipe samples in ug/%%ipe,soil and sludge samples in mg/kg and all TCLP and SPLP e\tracts <br /> in uglL <br /> "cluttered chromatogram sample peak coelutes urth surrogate peal. <br />' 'Ilte following descnpuons of the TPH chromatogram are cursory in nature and McCanipbell Analytical is not responsible for their <br /> interpretation a) unmodified or Acakly modified gasoline is significant b) heavier gasoline range compounds are significant(aged <br /> gasolme9) c) lighter gasoline range compounds (the most mobile fraction) are significant, d) gasoline range compounds baking broad <br /> chromatographic peaks are significant biologically altered gasoline? e)TPH pattern that does not appear to be derived from gasoline(9) 0 <br /> onc,to a feN+ isolated peaks present g)strongly aged gasoline or diesel range compounds are significant, h)lighter than eater immiscible <br /> sheen is resent i liquid sample that contains greater than—5 vol %sediment,i)no recognizable pattern <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />