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110 2nd Avenue South,#/D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> //www,mccaLphr.,ll com E-mail main@mccampbell com <br /> f <br /> ' Advanced GeoEnvironmental Client Project 1D Brolcides Petroleum Date Sampled 08/28/99 <br /> t4005 North Wilson Way Date Received 08/31/99 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 08/31-09/03/99 <br /> ' Client P O Date Analyzed 08/31-09/03/99 <br /> Oxygenated Volatile Organics By GC/AIS <br /> EPA method 8260 modified <br /> ' Lab ID 18247 18248 18249 18250 <br /> Reporting Limit <br /> Client 1D BMW 1 BMW 2 BMW 3 BWM 4 <br /> ' Matrix W W W W S W <br /> ' Compound Concentration* E. <br /> uglL <br /> Di-isopropyl Ether(D1PE) ND<3 5 ND<10 ND ND<25 50 to <br /> Ethyl tert-Butyl Ether(ETRE) ND<3 5 ND<10 ND ND<25 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) 130 380 44 170 50 10 <br /> ' tert-Amyl Methyl Ether(TAME) ND<3 5 ND<10 ND ND<25 50 10 <br /> tert-Butanol 33 ND<50 ND ND<130 25 50 <br /> Surrogate Recoveries(%) <br /> Dibramofluoromethane 100 106 99 99 <br /> ' Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysts <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than --5 vol %sediment, 0)sample diluted due to <br /> high organic content <br />' DHS Certification No 1644 1 Edward Hamilton, Lab Director <br />