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F <br /> Nf[NTViUi1yf VERIFICATION LABOR-A-TORY ANALYSIS , <br /> ` TPH-G iPH-D BTX +.4c E CL HC � TOTAi. titTBE �TALS PCB , <br /> TANK TAIN ICA-P/ 8270 <br /> R i CONTENTS 8015 8015 8020 8010 LEAD TBA, AES or gOgO <br /> P-60 8260 8260 8240 7420 RIPE, AA <br /> { 7421 ETRE, <br /> TAME <br /> 8260 <br /> I/ LEADED GAS X I x <br /> x x <br /> UNL GAS X x <br /> I DIESEL l x I x I I I <br /> KEROSENE I X X <br /> i. j <br /> I UNK FUEL x x r x x X <br /> PROD. OIL X x , <br /> I <br /> CHLOR. V <br /> ♦ X <br /> I <br /> SOLVENTS <br /> i <br /> � NONCHLOR X x I `� <br /> SOLVENTS <br /> h <br /> e WASTEI ; x X <br /> USED OIL l X x x x <br /> r <br /> r <br /> All analysis methods are the designated EPA methods described in EPA SW 846, Third Edition. Those rnerhods not found in <br /> ' SW 846 are speciitcally noted below. Refer to the "SWRCB LUFC Field Manual", Appendix D (B), Table 3-5 on page A26 for <br /> minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to 1-2-3 "l:eaiosaal Board Staff Recomrrsendatians <br /> Ffor Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> r <br /> I� L.-\BORATORY AINALYSES TER.NILNOLOGY-, <br /> T PH-G Total Petroleum Hydrocarbon, Gasoline. CC/FID (5030) 8415 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel. GC/FID (3550). 8015 mod or GCgviS 8260 <br /> r— BTX & E Benzene, Toluene. Xylene&Ethyl Benzene, GC;PID 8020 or GC/,,YiS 8260 <br /> CL HC Chlorinated Hydrocarbon. GC'HSD 8010, GCIMS 8240 <br /> TOTAL LEAD Total lead. AA 7420, AA 7421 or ICP-AES 6010 <br /> .ITBE,TANtE.D1PE.TBA GCIMS 8264 <br /> METALS IC.-�P or AA Inductively Coupled plasma Atomic Emission spectrometry 6010 or Arorni Absorption Spectrometry 7000• <br /> Metals: Cadmium, Chromium III and V1, Lead, Zinc and Nickel, <br /> PCB Polychlorinated Biphenyls. GCIMS 8270 or 8080 <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation, extraction method <br /> "tethod :034 Purge and trap Sample preparation <br /> QAIQC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detec on of benzene, benzene-free solvents are to be used, Fused capillary columns are preferred to packed <br /> columns-, a packed column may be used as a "first cut" with 'dirty" samples or once the hydrocarbons have been characterized and proper <br /> QA/QC is followed. <br /> For drinking water sources, EPA recommends that the 5W series for volatile organic should be used in preference to the 600 series because the <br /> detection limits are lower and the QAfQC is better. Samples exhibiting any level of heavy metal contamination may require Further analysis. <br /> PHS-EHD recommends holding those samples until disposal is indicated. <br /> F Page 8 <br /> EH 23 046 (Revised 10119/98) <br /> F <br />