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GeoAnalytical Laboratories , Inc. <br /> 2300 Maryann Dr. Turlock, CA 95380 Phone (209) 669-0100 Fax (209) 593-2212 <br /> email: la b.getr& tt.net <br /> Report # Y2K1601 Date: 11 /27/12 <br /> Jim Thorpe, Inc. Date Recd : 11 /16/ 12 <br /> P.O Box 357 <br /> Lodi, CA 95241 <br /> Volatile Organic Chemistry - Quality Control <br /> GeoAnalytical Laboratories, Inc. <br /> Reporting Spike Source %REC RPD <br /> Anal to Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch V003100 - EPA 5030 Prepared & Analyzed : 11/26/12 <br /> Matrix Spike (Y003100-MSI) _ Source: Y2K1601-03 <br /> Benzene 61 .2 5.0 ug/kg 60.00 ND 102 53-141 <br /> Di-isopropyl Ether (DIPE) 53.6 10.0 " 60.00 ND 89 68-134 <br /> Methyl tert-Butyl Ether (MTBE) 63.7 10.0 60.00 ND 106 76-179 <br /> Tert-Amyl Methyl Ether (TAME) 61 .4 10.0 60.00 ND 102 69-140 <br /> Toluene 57.8 5.0 It 60.00 ND 96 48-139 <br /> Gasoline 0.6 1 .0 mg/kg 1 .500 ND 39 63-143 S-LOW <br /> Surrogate: 1, 2-Dichloroelhane-d4 21.8 ug/kg 20. 00 log 72-132 <br /> Surrogate: 2-Broma- l-Chloroprpane 15.2 It 20.00 76 71434 <br /> Surrogate: 4-Bromfluoroben-ene 18, 3 If 20.00 92 74-132 <br /> Surrogate: 1.2-Dlchloroethane-d4 0.0213 mg/kg 0. 02000 107 72-132 <br /> Surrogate: 2-Bramo-l-Chlorpropane 0. 0153 0o2000 76 71-134 <br /> Surrogate: 4-Bromrfluarobemene 0. 0196 IF0:02000 98 74-132 <br /> Matrix Spike Dup (Y003100-MSDI) Source: Y21K1601-03 <br /> Benzene 614 5.0 ug/kg 60,00 ND 102 53-141 0.4 20 <br /> Di-isopropyl Ether (DIPE) 52.4 10.0 IF 60.00 ND 87 68- 134 2 20 <br /> Methyltert-Butyl Elhcr (M1"BE) 644 10,0 Is 60.00 ND 107 76- 179 1 28 <br /> Tert-Amyl Methyl Ether ('TAME) 62.7 10,0 " 60.00 ND 104 69- 140 2 19 <br /> Toluene 59.4 5.0 " 60.00 ND 99 48-139 3 24 <br /> Gasoline 0.5 1 .0 mg/kg 1 .500 ND 36 63-143 9 34 S-LOW <br /> Surrogate: 1,2-Dichloroetbane-d4 12,4 uglkg 20.00 112 72-132 <br /> Surrogate. 2-Bromo-l-Chloropropane 15.5 It20.00 77 71434 <br /> Surrogate: 4-Brom fluoroben-ene 19. 8 if20. 00 99 74-132 <br /> Surrogate: 1,2-Dichloroelhane-d4 0. 0220 mg/kg 0.01000 710 72-132. <br /> Surrogate: 2-Brcmo4-Chloropropane 0.0156 IF 0.02000 78 71434 <br /> Surrogate: 4-Brom qfluoroben:ene 0. 0193 it 0. 02000 96 74-132 <br /> Certification # 2595 <br />