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d <br /> Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431 -5778 <br /> (775) 3554044 • (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: QC Summary Report W140 04`42 <br /> 13-Mar-14 <br /> Method Blank Type MBLK Test Code: EPA Method SW6020I SW6020A <br /> File ID: 030_ Batch ID: 32632 Analysis Date: 031051201411 :42 <br /> Sample ID: MB-32632 Units : mglKg Run ID: ICPIMS_1403068 Prep Date: 031042014 1 4:49 <br /> Analyte Result PRL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Limlt) Qual <br /> Lead (Pb) ND t <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW60201 SW6020A <br /> File ID: 032_ Batch ID: 32532 Analysis Date: 031061201411 :46 <br /> Sample ID: LCS42632 Units : mglKg Run ID: ICPIMS_140305B Prep Date: 031041201414:49 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRetVal %RPD(Llmlt) Qual <br /> Lead (Pb) 25.6 1 25 102 80 120 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW6020I SW6020A <br /> File ID: 034_ Batch ID: 32532 Analysis Date: 031051201411 :64 <br /> Sample ID: 1402272241AMS Units : mgtKg Run ID: ICPIMS 740306B Prep Date: 031041201414:49 <br /> Analyte - Result PQL SpkVal SpkRefVal %REC LCL(ME_) UCL(ME) RPDRefVal %RPD(Limit) Qua] <br /> Lead (Pb) 33.1 1 . 25 9.715 94 75 125 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW60201 SW6020A - <br /> File ID: 035_ Batch ID: 32532 Analysis Date: 0310 512 014 11 :51 <br /> Sample ID: 14022722,01AMSD Units : mg/Kg Run ID: ICPIMS_140305B Prep Dale: 0310412014 14:49 <br /> AnalyteResult PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME) RPDRefVal %RPD(Umit) Qual <br /> Lead (Pb) 34.5 1 25 9.715 99 75 125 33.15 4.1(20) <br /> Comments: <br /> Calculations are based off of mw (non-rounded) data However, For reporting purposes, all QC data is rounded to three significant figures. Therefore, hand calculated <br /> values may differ slightly. <br />