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Appendix 8 - Standard Operating Procedures <br /> Page 2 of 2 <br /> Updated 08/1/2014 a ntea g ro u p <br /> Organic Vapor Procedures <br /> Soil samples are collected for analysis in the field for ionizable organic compounds using a photo-ionization detector (PID). <br /> The test procedure involves measuring approximately 30 grams from an undisturbed soil sample, placing this sub-sample <br /> j in a Zip-type bag or foil-wrapped jar. The container is warmed for approximately 20 minutes in the sun, then the head- <br /> space within the container is tested for total organic vapor measured in parts per million as benzene (ppm; <br /> volume/volume). The instrument is calibrated prior to drilling. The results of the field-testing are notedon the boring <br /> logs. PID readings are useful as a qualitative indication of relative levels of contamination, but cannot be used to quantify <br /> i <br /> petroleum hydrocarbon concentrations with the confidence of laboratory analyses. <br /> Equipment Decontamination <br /> Equipment that could potentially come in contact subsurface media and compromise the integrity of the samples is <br /> carefully decontaminated prior to drilling and sampling. Drilling auger and other large pieces of equipment are <br /> decontaminated using high pressure hot water spray. Soil and groundwater sampling apparatus, groundwater pumps, <br /> liners and other equipment are decontaminated in an Alconox scrub solution and double rinsed in clean tap water rinse <br /> followed. by a final distilled water rinse. <br /> The rinsate and other wastewater are contained in 55-gallon DOT-approved drums, labeled (to identify the contents, <br /> generation date and project) and stored on-site pending waste profiling and disposal. <br /> Waste Handling and Disposal (Soil Cuttings and Rinsate/Purge Water) <br /> Soil cuttings and rinsate/purge water generated during drilling and sampling are stored on-site in DOT-approved 55-gallon <br /> steel drums pending characterization. . A label is affixed to the drums indicating the contents of the drum, suspected <br /> contaminants, date of generation, and the boring number from which the waste is generated. The drums are removed <br /> from the site by a licensed waste disposal contractor to an appropriate facility for treatment/recycling. <br />