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. , . • • <br /> QC Sample Results <br /> Client: Bureau Veritas North America, Inc. TestAmerica Job ID:720-415814-1 t <br /> Project/Site: Lodi Verizon V011.>sn <br /> Method: 8260B -Volatile Organic Compounds(GCIMS)(Continued) -I <br /> Lab Sample ID:720-45814-5 MSD Client Sample ID: B3-2'-2.5' <br /> Matrix:Solid Prep Type:Total/NA <br /> Analysis Batch: 124880 Prep Batch: 124903 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Trichlorofluoromethane ND 50.0 51.3 ug/Kg 103 61---130 2 20 <br /> _.._.._ _ <br /> 1,2,3Tdchloropropane ND 50.0 59.1 ug/Kg 118 62.150 4 20 <br /> 1,1,2-Tnchloro-1,2,2-trifluoroetha ND 50.0 53.0 ug/Kg 106 52-130 5 20 <br /> re <br /> 1,2,4-Trimethylbenzene ND 50.0 54.9 ug/Kg 110 64.140 7 20 + w <br /> 1,3,5-Tdmethylbenzene ND 50.0 54.8 ug/Kg 110 67-134 7 20 << . <br /> Vinyl acetate ND 50.0 ND F ug/Kg 30 52.150 25 20 <br /> Vinyl chloride ND 50.0 48.1 ug/Kg 96 62-130 6 20 <br /> m-Xylene 8 p-Xylene ND 100 116 ug/Kg 116 70-130 5 20 <br /> c-Xylene ND 50.0 57.7 ug/Kg 115 68-130 5 20 <br /> 2,2-Dichloropropane ND 50.0 65.9 F ug/Kg 132 63-130 3 20 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromolluorobenzene 107 46.131 <br /> 1,2-Dichloroethane-d4(Sum) 99 60-140 <br /> Toluene-d8(Sun) 104 58-140 <br /> Method: 80156-Diesel Range Organics(DRO) (GC) <br /> Lab Sample ID:MB 720-124893/1-A Client Sample ID: Method Blank <br /> Matrix:Solid Prep Type:Silica Gel Cleanup <br /> Analysis Batch: 124913 Prep Batch: 124893 <br /> me Me <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Diesel Range Organics[C70-C28] ND 0.98 m9/K9 11/08/1219:42 11/09/1213:32 1 <br /> Motor Oil Range Organics[C24-C36] ND 49 mg/Kg 11/08/1219:42 11/09/1213:32 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Llmlfs Prepared Analyzed oil Fee <br /> Capdc Acid(Surr) 0.002 0-1 <br /> —FI/—Oa/1219:42 11/09/1213:32 i <br /> p-Terphenyl 105 38-148 11/0811219:42 11109/1213:32 1 <br /> Lab Sample ID: LCS 720-12489312-A Client Sample ID:Lab Control Sample <br /> Matrix:Solid Prep Type:Silica Gel Cleanup <br /> Analysis Batch: 124913 Prep Batch: 124893 <br /> Spike LCS LCs %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> Diesel Range Organics 82.2 56.1 mg/Kg 68 36-112 <br /> [C10-C28] <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> p-Terphenyl 96 38.148 <br /> Lab Sample ID: LCSD 720-124893/3-A Client Sample ID: Lab Control Sample Dup <br /> Matrix:Solid Prep Type:Silica Gel Cleanup <br /> Analysis Batch: 124913 Prep Batch: 124893 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Diesel Range Organics 82.2 59.9 mg/Kg 73 36-112 7 35 <br /> [CIO-C28] <br /> TestAmerica Pleasanton <br /> Page 20 of 30 11/13/2012 <br />