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Entech Analytical Labs, Inc , Santa Clara, CA <br /> Lab Report No H3021711 Date 02/27/2003 Page 3 <br /> Project Name CARDOZA Analysis Volatile Organic Compounds by GC/MS Fuel <br /> Project No 6622 Method 8260FA <br /> Prep Meth SW5030B <br /> ' Field ID MW-2 Lab Samp ID 33375-001 <br /> Descr/Location MW-2 Recd Date 02/19/2003 <br /> Sample Date 02/13/2003 Prep Date 02/20/2003 <br /> Sample Time 0810 Analysis Date 02/20/2003 <br /> Matrix Water QC Batch WMS11943 <br /> Basis Not Filtered Notes <br /> ' Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Methyl-tent-butyl ether(MTBE) 03 1 PQL ND UG/L 1 <br /> ' Ethyl tert-butyl ether(ETBE) 05 5 PQL ND UG/L 1 <br /> tert-Amyl methyl ether(TAME) 03 5 PQL ND UG/L 1 <br /> Di-isopropyl ether (DIPE) 05 5 PQL ND UG/L 1 <br /> ' tert-Butyl alcohol (TBA) 46 10 PQL ND UG/L 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES <br /> 4-Bromofluorobenzene 65-135 SMEA 111% i <br /> Toluene-d8 77-150 SMSA 120% i <br /> Dibromofluoromethane 57-156 SMEAAZ 194% 1 1 <br /> AZ Surr recovery outside of acceptance limits due to matrix interf <br /> 1 <br /> Approved by <br /> Date 2' � <br /> I <br />