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E <br /> E Entech Analytical Labs, Inc:, Santa Clara, CA <br /> .-.� Lab Report No.: H212161Z Date: 12/2612002 Page: 3 <br /> Project Name: SUPER STOP MARKET Analysis: Volatile Organic Compounds by GC/MS Fuel <br /> Project No: 662.2 Method: 8260FA <br /> Prep Meth: SW5030B <br /> Field ID: MW-2 Lab Samp ID: 32600-004 <br /> Deser/Location: MW-2 Recd Date: 12/18/2002 <br /> Sample Date: 12/13/2002 Prep Date: 12/19/2002 <br /> Sample Time: 1237 Analysis Date: 12/19/2002 <br /> Matrix: Water QC Batch: WMS11850 <br /> Basis: Not Filtered Notes: <br /> Analyte Det Limit Rep Limit Note Result Units Pvc Dil <br /> Met yl-cert-butyl ether(MTBE) 0.3 1. PQL ND UG/L 1 <br /> Ethyl tent-butyl ether(ETBE) 0.5 5. PQL ND UGIL 1 <br /> tert-Amyl methyl ether(TAME) 0.3 5. PQL ND UG/L 1 <br /> Di-isopropyl ether(DIPS) 0.5 5. PQL ND UGIL 1 <br /> tert-Butyl alcohol (TBA) 1 4.6 10. PQL ND UGIL 1 <br /> SURROGATE AND INTERNAL STANDARD RECOVERIES: <br /> 4-Bromotluorobenzene 65-135 SMEA 114% 1 <br /> Toluene-d8 77-150. SMEA 118% 1 <br /> Dibromofluoromethane 57-156 SMEAAZ 8.9% ! 1 <br /> AZ: Surr. recovery outside of acceptance limits due to matrix interl. <br /> i <br /> I <br /> Approved by: U , Date: yr 7T�1�. <br /> �I <br />