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Alpha Analytical, Inc. <br /> 255 Glendale Ave. - Suite 21 - Sparks,Nevada 89431-5778 <br /> (775)355-1044 -(775)355-0406 FAX - 1-800-283-1183 <br /> ate: Work Order: <br /> u -03 QC Summary Report 03072924 <br /> Method Blank - Type MBLK Test Code: EPA Method SW826013 <br /> File ID: D:IHPCHEM1MS09IDATAI03D801103080107.D Batch ID:MS9W0801A Analysis Date: 0810112003 10:22 <br /> Sample ID: MBLK MS9WO801A Units:pg1L Run ID:GCIMSD 8_030801A Prep Date: 08/0112003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-imit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol {TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETRE) ND 1 <br /> Benzene ND 0.5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene ND 0.5 <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr: 1,2-Dichloroethane-d4 9.35 10 94 72 126 <br /> Surr:Toluene-d8 10.3 10 103 71 128 <br /> Surr:4-Bromofluorobenzene 9.82 10 98 76 121 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEM1MS091DATA1030B01103080105.D Batch ID:MS9WO801A Analysis Date: 08101/2003 09:38 <br /> Sample ID: LCS MS9WO801A Units:pg1L Run ID:GCIMSD_9_030801A Prep Date: 08101/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 9.69 0.5 10 97 83 119 <br /> Toluene 9.95 0.5 10 100 80 120 <br /> Ethylbenzene 10 0.5 10 100 80 120 <br /> m,p-Xylene 19.7 0.5 20 99 77 124 <br /> o-Xylene 9.97 0.5 10 99.7 77 125 <br /> rr: 1,2-Dichloroethane-d4 9.42 10 94 72 126 <br /> wrrToluene-d8 10.4 10 104 71 128 <br /> :4-Bromofluorobenzene 10.2 10 102 76 121 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: D:IHPCHEM1MS091DATA1030601103080109.D Batch-ID:MS9WO801A Analysis Date: 08101/2003 11:08 <br /> Sample ID: 03072823-OBAMS Units:pg1L Run ID:OCIMSD_9_030801A Prep Date: 06101/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 46.8 1.3 50 0 94 83 199 <br /> Toluene 48.6 1.3 50 0 97 80 120 <br /> Ethylbenzene •49.3 1.3 50 0 99 80 120 <br /> m,0-Xylene 96.3 1.3 100 0 96 77 124 <br /> o-Xyiene 48.5 1.3 50 0 97 77 125 <br /> Surr: 1,2-Dichloroethane-d4 46.2 50 92 72 126 <br /> Surr:Toluene-d8 50.5 50 101 71 928 <br /> Surr:4-Bromofluorobenzene 51.3 50 103 76 921 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SWB260B <br /> File ID: D:IHPCHEMIMS091DATA1030801103DB0110.D Batch ID:MS9W0801A Analysis Date: 08/01/2003 11:30 <br /> Sample ID: 03072823-OBAMSD Units:pgIL Run ID:GCIMSD_9_030801A Prep Date: OBIDII2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 45.5 1.3 50 0 91 83 119 46.75 2.82 <br /> Toluene 47 1.3 50 0 94 80 120 48.63 3.32 <br /> Ethylbenzene 47.2 1.3 50 0 94 80 120 49.25 4.21 <br /> m,p-Xylene 93.4 1.3 100 0 93 77 124 96.31 3.1 <br /> =o=Xylene -_ __ - -_- -- 47.1 . --1.3 50 - ---- 0 94 77 - <br /> -125. 48.47 - - 2.89 -- - - <br /> Surr: 1,2-Dichloroethane-d4 46.4 50 93 72. 126 <br /> Surr:Toluene-d8 50.9 50 102 71 128 <br /> Surr:4-Bromofluorobenzene 51.6 50 103 76 121 <br /> mments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> 13.Analyte detected in the associated Method Blank. <br />