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Alpha Analytical, Inc. 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 (775)355-1044 •(775) 355-0406 FAX• 1-800-283-1183 Date: z1-Apr-03 QC Summary Report Work Order: 0304[12] Method Blank Type MBLK Test Code: EPA Method SW8260B File ID: D:kHPCHEMkMS09IDATAI030414103041407,D Batch ID: MS9W0414A Analysis Date: 04/14/2003 10:40 Sample ID: MBLK MS9W0414A Units : pg1L Run ID:GCIMSD_9_030414A Prep Date: 04114/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Quai Tertiary Buty)Alcohol(TBA) ND 5 Methyl tert-butyl ether(MTBE) ND 0.5 Di-isopropyl Ether(DIPS) ND 1 Ethyl Tertiary Butyl Ether(ETBE) ND 1 Benzene ND 0.5 Tertiary Amyl Methyl Ether(TAME) ND 1 Toluene ND 0.5 Ethylbenzene ND 0.5 m,p-Xylene ND 0.5 o-Xylene ND 0.5 Surr: 1,2-Dichloroethane-d4 9.08 10 91 71 130 Surr:Toluene-d8 10.4 10 104 69 127 Surr:4-Bromofluorobenzene 9.32 10 93 80 123 Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B File ID: D:IHPCHEM1MS091DATA1030414103041405.D Batch ID: MS9W0414A Analysis Date: 04/14/2003 09:54 Sample ID: LCS MS9W0414A Units: }tg1L Run ID:GC/MSD_9_030414A Prep Date: 04114/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual Benzene 9.86 0.5 10 99 80 120 Toluene 10.4 0.5 10 104 80 120 Ethylbenzene 10.7 0.5 10 107 80 120 m,p-Xylene 19.2 0.5 20 96 73 129 --Xylene 9.65 0.5 10 97 73 127 -r: 1,2-Dichloroethane-d4 8.73 10 87 71 130 %wa,trr:Toluene-d8 10.4 10 104 69 127 Surr:4-Bromofluorobenzene 10.2 10 902 80 123 Sample Matrix Spike Type MS Test Code: EPA Method SW82608 File ID: D:IHPCHEMIMS09%DATAk03O4l4kO3O4l4l O.D Batch iD: MS9W0414A Analysis Date: 04/14/2003 11:52 Sample ID: 03041121-OIAMS Units! pg1L Run ID:GC/MSD_9_030414A Prep Date: 04/14/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual Benzene 45 1.3 50 0 90 80 120 Toluene 47.5 1.3 50 0 95 80 120 Ethylbenzene 49.1 1.3 50 0 98 80 120 m,p-Xylene 89.3 1.3 100 0 89 73 129 o-Xylene 44.6 1.3 50 0 89 73 127 Surr:1,2-Dichloroethane-d4 43.6 50 87 71 130 Surr:Toluene-d8 52.1 50 104 69 127 Surr 4-Bromofluorobenzene 49.2 50 98 80 123 Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B File 1D: D:IHPCHEMIMS091DATA1030414103041411.D Batch ID: MS9W0414A Analysis Date: 04/14/2003 12:15 Sample Q 03041121-01AMSD Units: pg/L Run ID:GCIMSD_9_030414A Prep Date: 04/14/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual Benzene 43.1 1.3 50 0 86 80 120 44,96 4.2 Toluene 46.2 1.3 50 0 92 80 120 47,49 2.8 Ethylbenzene 47.7 1.3 50 0 95 80 120 49.11 3.02 m,p-,Xylene 88 1.3 100 0 88 73 129 89.3 1.42 o-Xylene 43.5 1.3 50 0 87 73 127 44,63 2.47 Surr: 1,2-Dichloroethane-d4 43.8 50 88 71 130 Surr: Toluene-d8 52.7 50 105 69 127 Surr: 4-Bromofluorobenzene 50.4 50 101 80 123 " nments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank.