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Date- <br /> Alpha Order- <br /> 01050723�s-May-o� Alpha Analytical, Inc. - QC Summary Report 01050723 <br /> Method $lank Type MBLK Test Code: SW8260B Batch ID:MS8S0510A <br /> File ID:D:IHPCHEM1MS081DATA1010510101051014.D Analysis Date: 05110/2001 16:28 <br /> OSample ID: MBLK MSBS0510AIB Units:trglKg Run ID:GC/MS D_$_010510A Prep Date: 05/10/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Tertiary Butyl Alcohol (TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 20 <br /> 1,2-Dichloroethane ND 20 <br /> Benzene ND 5 <br /> Tertiary Amy) Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr. 1,2-Dichloroethane-d4 207 200 104 65 135 <br /> Surr:Toluene-d8 189 200 94 65 135 <br /> Sum 4-Bromofluorobenzene 231 200 116 65 135 <br /> Laboratory Control Spike Type LCS Test Code:SW8260B Batch ID:MSSS0510A <br /> File ID: D;IHPCHEM1MS081DATA1010510101051044.D Analysis Date: 05/11/2001 05:37 <br /> Sample ID: LCS MSOS0510A Units:pg/Kg Run ID:GC/MSD_6_010510A Prep Date: 05/11/2001 <br /> Analyte Result PQL Spkval SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qua] <br /> Methyl tert-butyl ether(MTBE) 471 5 200 85 65 135 <br /> Benzene 189 5 200 95 65 135 <br /> Toluene 186 5 200 93 65 135 <br /> Ethylbenzene 187 5 200 93 65 135 <br /> m,p-Xylene 371 5 400 93 65 135 <br /> o-Xylene 190 5 200 95 65 135 <br /> Surr: 1,2-Dichloroethane-d4 184 200 92 65 135 <br /> Surr:Toluene-d8 195 200 97 65 135 <br /> Surr:4-Bromofluorobenzene 215 200 107 65 135 <br /> ample Matrix Spike Type MS Test Code: SW8260B Batch ID:MSSS0510A <br /> ile ID:D:IHPCHEM1MS08XDATA1010510101051046.D Analysis Date: 05/11/2001 06:30 <br /> Sample ID: 01051066-06AMS Units:pg/Kg Run ID:GC/MSD_8_010510A Prep Date: 05/11/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 391 10 400 0 98 65 135 <br /> Benzene 374 10 400 0 94 65 135 <br /> Toluene 356 10 400 0 89 65 135 <br /> Ethylbenzene 367 10 400 0 92 65 135 <br /> rn,p-Xylene 739 10 800 0 92 65 135 <br /> o-Xylene 383 10 400 0 96 65 135 <br /> Surr: 1,2-Dichloroethane-d4 353 400 88 65 135 <br /> Surr:Toluene-d8 377 400 94 65 135 <br /> Surr:4-Bromofluorobenzene 425 400 106 65 135 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: SW8260B Batch ID:MSBS0510A <br /> File ID:D;IHPCHEMkMSOB1DATAW10510101051047.D Analysis Date: 05/1112001 06:56 <br /> Sarnple ID: 01051066-06AMSD Units:pg/Kg Run 1D:GC/MSD^8_010510A Prep Date: 05/11/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPI) Qual <br /> Methyl tent-butyl ether(MTBE) 397 10 400 0 99 65 135 391.5 1.33 <br /> Benzene 411 10 40D 0 103 65 135 374.5 9.41 <br /> Toluene 393 10 400 0 98 65 135 356.3 9.79 <br /> Ethylbenzene 404 10 400 0 101 65 135 366.6 9.71 <br /> m,p-Xylene 817 10 800 0 102 65 135 738.6 10.1 <br /> o-Xylene 419 10 400 0 105 65 135 383.1 8.99 <br /> Surr: 1,2-Dichloroethane-d4 359 400 90 65 135 <br /> Surr.Toluene-d8 378 400 95 65 135 <br /> Surr:4-Bromofluorobenzene 421 400 105 65 135 <br /> Comments: ND-Not Detected at the Reporting Limit. D- if the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br />