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16-May-01 Alpha Analytical, Inc. - QC Summary Report Work Order: <br /> 01050724 <br /> Method Blank Type MBLK Test Code: SW8015 Batch ID:MSBS0510B <br /> File ID:D:IHPCHEMIMS08IDATAID10510101051014.D Analysis Date: 05/10/2001 16:28 <br /> Sample ID: MBLK MS8S0510A/B Units :mglKg Run ID:GCIMSD_8 010510A Prep Date: 05/10/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPI`-[ Purgeable ND 1 <br /> Surr: 1,2-Dichloroeth2ne-d4 0.207 0.2 104 65 135 <br /> Surr:Toluene-d8 0.189 0.2 94 65 135 <br /> Surr:4-Bromofluorobenzene 0.231 0.2 116 65 135 <br /> Laboratory Control Spike Type LCS Test Code: SW8015 Batch ID:MSBS0510B <br /> File ID:D:IHPCHEM1MS081DATA1010510101051045.D Analysis Date: 05/11/2001 06:04 <br /> Sample ID: GLCS MSBS0510113 Units :mglKg Run ID:GCIMSD_8_010510A Prep Date: 05/11/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 6.04 1 8 75 61 144 <br /> Surr: 1,2-Dichloroethane-d4 0.185 0.2 92 65 135 <br /> Surr.Toluene-d8 0.189 0.2 94 65 135 <br /> Sum 4-Bromofluorobenzene 0.196 0.2 98 65 135 <br /> Sample Matrix Spike Type MS Test Code: SW8015 Batch ID:MSBS05108 <br /> File 0: 0:IHPCHEMIMS081DATA1010510101051048.D Analysis Date: 05/111200107:23 <br /> Sample ID: 01051066-07AGS Units :mglKg Run ID:GCIMSD_8_010510A Prep Date: 05/11/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 12.7 2 16 0 79 61 144 <br /> Surr: 1,2-Dichloroethane-d4 0.366 0.4 92 65 135 <br /> Surr:Toluene-d8 0.374 0.4 93 65 135 <br /> Surr:4-Bromofluorobenzene 0.384 0.4 96 65 135 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: SW8015 Batch ID:MS8S0510B <br /> File ID: D:IHPCHEMIMS081DATA1010510101051049.D Analysis Date: 05/11/2001 07:49 <br /> Sample ID: 01051066-07AGSD Units :mg1Kg Run ID:GCIMSD_8_010510A Prep Date: 05/91/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Re(Val %RPD Qual <br /> wTPH Purgeable 15.2 2 16 0 95 61 144 12.65 18.3 <br /> Surr: 1,2-Dichloroethane-d4 0.371 0.4 -93 65 135 <br /> Surr.Toluene-c!8 0.368 0.4 92 65 135 <br /> Surr:4-Bromofluorobenzene 0.387 0.4 97 65 135 <br /> Comments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br /> i <br />