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Date: ; Order: <br /> 08-Mar-01 Alpha Analytical, In. - C Sunnna�Y Report 01022794 <br /> Method Wank Test Code: SW6260B Batch ID: MS4W0301A Analysis Date: 03101/2001 12:13 <br /> Sample ID: MBLK MS4W0301A Units:pglL Run ID:GC/MSD_4_010301A Prep Date: 0310112001 <br /> Analyte Result PQL SpkVal SpkRefdal %REC Lowl-imit HighLimit RPD Ref Vai %RPD Qual <br /> Tertiary Butyl Alcohol(TBA) ND 10 <br /> Methyl tert-butyl ether(MTBE) ND 0.5 <br /> Di-isopropyl Ether(DIPE) ND 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 1 <br /> Benzene NO 0.5 <br /> Tertiary Amyl Methyl Ether(TAMC) ND 1 <br /> Toluene ND M <br /> Ethylbenzene ND 0.5 <br /> m,p-Xylene ND 0.5 <br /> o-Xylene ND 0.5 <br /> Surr. 1,2-Dichloroethane-d4 9.47 10 95 70 130 <br /> Surr:Toluene-d8 9.83 10 98 70 130 <br /> Sum 4-Bromot5uorobenzene 10.5 10 105 70 130 <br /> Laboratory Control Spike Test Code: SVVB2605 Batch ID: M34WO301A Analysis Date: 03101;2001 15:43 <br /> Sample ID: LCS MS4W0301A Units:pglL Run ID:GCIMSt?_4_010301A Prep Date: 03/01/2001 <br /> Analyte Result PQL SpkVal SpkRefVal %R:-;'C Lowl-im4 HighLimit RPD Ref Val %RPD Qual <br /> Methyl teri-butyl ether(MT3H) 9.68 0.5 10 97 70 130 <br /> Benzene 10.5 0.5 10 105 70 130 <br /> Toluene 10.3 0.5 10 103 70 130 <br /> Ethylbenzene 10.1 0.5 10 101 70 130 <br /> m,p-Xylene 21.9 0.5 20 110 70 130 <br /> o-Xylene 10.4 0.5 10 104 7D 130 <br /> Surr: 1,2-Dichloroethane-d4 9.53 10 95 70 130 <br /> Surr:Toluene-d8 9.86 10 99 70 130 <br /> Surr:4-Bromofiuorobenzene 10.7 10 107 70 130 <br /> Sample Matrix Spike Test Code: SW6260B Batch ID: MS4W0301A Analysis Date: 0310512001 21:33 <br /> Sample ID: 01022762-01AMS Units:pg1L Run ID:GCIMSD_4_010301A Prep Date: 0310512001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Methyi tert-butyl ether(MTBE) 44.3 2.5 50 0 89 70 130 <br /> Benzene 51.4 2.5 50 0 103 70 130 <br /> Toluene 51.1 2.5 50 0 102 70 130 <br /> Ethylbenzene 46.5. 2.5 50 0 93 70 130 <br /> m,p-Xylene 101 2.5 100 0 101 70 130 <br /> o-Xylene 47 2,5 50 0 94 70 130 <br /> Surr: 1,2-Dichlorosth2ne-d4 45.1 50 90 70 130 <br /> Surr:Toluene-d8 52 50 104 70 130 <br /> Surr:4-Bromofiuorobenzene 55.1 50 110 70 130 <br /> Sample Matrix Spike Duplicate Test Code: SW6260B Batch ID: MS4W0301A Analysis Date: 03/05/2001 21:54 <br /> Sample ID: 01022762-01AMSD Units :pg/L Run 1D:GCIMSD_4_010301A Prep Date: 0310512001 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> Methyl tert-butyl ether(MTBE) 42.5 2.5 50 0 85 70 130 44.34 4,35 <br /> Benzene 49.2 2.5 50 0 98 70 130 51.38 4,38 <br /> Toluene 49.1 2.5 50 0 98 70 130 51.09 3.97 <br /> Ethylbenzene 45.4 2.5 50 0 91 70 130 45.48 2.28 <br /> m,p-Xylene 97.3 2.5 100 0 97 70 130 101.1 3.76 <br /> o-Xylene 45.8 2.5 50 0 92 70 130 46.99 2.61 <br /> Surr: 1,2-Dichloroeth2ne-d4 44.1 50 85 70 130 <br /> Surr:Toluene-d8 51.5 50 103 70 130 <br /> Sum 4-Bromofiuorobenzene 54 50 10B 70 130 <br /> Comments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not he calculated <br /> S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. <br /> B-Analyte detected in the associated Method Blank. <br /> • <br /> .... <br />