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1 <br /> Alpha Analytical, Inc. <br /> l 255 Glendale Ave. •Suite 21 •Sparks,Nevada 89431-5778 <br /> l� (775) 355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> te' Work Order: <br /> an-ops OC Summary Report <br /> 06010655 <br /> Method Blank Type:MBLK Test Code:EPA Method SW8260B <br /> File 10: D:IHPCHEM1MS101DATA1060111106011107.D Batch 0:MSI 0A0111A Analysis Date: 01/11/200609:32 <br /> Sample ID: MBLK MS10A0111A Units:mg/m3 Run ID:MSD_10_050111A Prep Date: 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 5 <br /> Methyl tert-butyl ether(MTBE) ND 0.1 <br /> Di-isopropyl Ether(DIPS) ND 0.2 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 0.2 <br /> Benzene ND 0.1 <br /> Tertiary Amyl Methyl Ether(TAME) ND 0.2 <br /> Toluene ND 0.1 <br /> Ethyibenzene ND 0.1 <br /> m,p-Xylene ND 0.1 <br /> o-Xylene ND 0.1 <br /> Surr: 1,2-Dichloroethane-d4 1.82 2 91 76 127 <br /> Surr:Toluene-d8 1.77 2 89 84 113 <br /> Surr:4-Bromofluorobenzene 2.07 2 104 79 119 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW8260B <br /> He 1D:D:IHPCHEMWIS101DATA1060111106011104.D Batch ID:MSI 0A0111A Analysis Date: 011111200608:27 <br /> Sample ID: LCS MSI 0A0111A Units:mg/m3 Run ID:MSD_10_060111A Prep Date: 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowi_imit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Benzene 10 0.1 10 100 81 122 <br /> Toluene 9.6 0.1 10 96 80 120 <br /> Ethylbenzene 9.82 0.1 10 98 80 120 <br /> m,p-Xyiene 10.1 0.1 10 101 80 129 <br /> o- Iene 9.67 0.1 10 97 80 129 <br /> 1,2-Dichloroethane-d4 10.7 10 107 76 127 <br /> Toluene-d8 9.47 10 95 84 113 <br /> Surr:4-Bromofluorobenzene 9.79 10 98 79 119 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />