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ALAlpha Analytical, Inc, <br /> 255 GIendale Ave. •Suite 21 •Sparks,Nevada 84431-5778 <br /> (775)355-1044 •(775) 355-0406 FAX• 1-800-283-1183 <br /> We-.06 <br /> Work Order: <br /> OC Summary Report 06011003 <br /> Method Blank Type:MBLK Test Code:EPA Method SW8260B-Dl <br /> File ID:C:IHPCHEMIMS111DATA1060111106011103.D Batch ID:13885 Analysis Date: 0111 112006 10:28 <br /> Sample 1D: MBLK-13885 Units:}rg/L Run ID:MSD_i 1_060111A Prep Date. 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limlt) Qual <br /> Methanol ND 5000 <br /> Ethanol ND 5000 <br /> Surr:Hexafluoro-2-propanol 508 500 102 63 137 <br /> Laboratory Control Spike Type:LCS Test Code:EPA Method SW826013-113I <br /> File ID:C.-XHPCHEM1MS11�DATA�060111�06011104.D Batch ID:1388S Analysis Date: 01/11/2006 10:49 <br /> Sample ID: LCS-13885 Units,pg/L Run ID:MSD_11_060111 A Prep Date: 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Methanol 261 50 250 104 45 155 <br /> Ethanol 251 5 250 100 51 144 <br /> Surr:Hexafluoro-2-propanol 490 500 98 63 137 <br /> Sample Matrix Spike Type:MS Test Code:EPA Method SW82606-DI <br /> File ID:C:IHPCHEM1MS111DATA1060111\06011106.D Batch ID:13885 Analysis Date: 01111/2006 11:30 <br /> Sample ID: 06011003-02AMS Units:yglL Run ID:MSD_11_060111A Prep Date: 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Methanol 257 50 250 0 103 45 163 <br /> Ethanol 255 5 250 0 102 50 149 <br /> Surr.Hexafluoro-2-propanol 511 500 102 63 137 <br /> Sample Matrix Spike Duplicate Type:MSD Test Code:EPA Method SW826013-0 <br /> *F ID:C:XHPCHEMXMS111DATAko6oliiXo6ollio7.0 Batch ID:13885 Analysis Date: 01/1112006 11:50 <br /> le ID: 06011003-02AMSD Units:Ng/L Run ID:MSD_11_060111A Prep Date: 01/11/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Methanol 226 50 250 0 90 45 163 257.2 13.1(22) <br /> Ethanol 240 5 250 0 96 50 149 255.1 6.1(15) <br /> Surr:Hexafluoro-2-propanol 509 500 102 63 137 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per liter,per client request. <br />