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Alpha Analytical, Inc. p ( I 255 Glendale Ave. •Suite 21 - Sparks,Nevada 89431-5778 (775) 355-1044 - (775) 355-0406 FAX - 1-800-283-1183 Date: 24-Jan-03 QC Summary Report Work Order: 03012224 Method Blank Type MBLK Test Code! EPA Method SW8260B File ID: D:IHPCHEMIMS101DATA1030123103012306.D Batch ID: MS10WO123A Analysis Date: 01/23/2003 09:40 Sample ID: MBLK MSIOW0123A Units : pg/L Run ID:GCIMSD_10_030123A Prep Date: 01/2312003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hightimit RPD Ref Val %RPD Qual Tertiary Butyl Alcohol (TBA) NO 5 Methyl tert-butyl ether(MTBE) NO 0.5 Di-isopropyl Ether(DIPE) ND 1 Ethyl Tertiary Butyl Ether(ETBE) NO 1 Benzene NO 0.5 Tertiary Amyl Methyl Ether(TAME) ND 1 Toluene ND 0.5 Ethylbenzene NO 0.5 m,p-Xylene NO 0.5 o-Xylene NO 0.5 Surr: 1,2-Dichloroethane•d4 10.9 10 109 71 130 Surr:Toluene-d8 9.86 10 99 69 127 Surr: 4-Bromofluorobenzene 9.74 10 97 80 123 Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B File 1D: D:IHPCHEMIMSIOIDATA1030123103012304.D Batch ID: MS10WO123A Analysis Date: 01/23/2003 08:57 Sample ID: LCS MSIOW0123A Units : pg1L Run ID:GC/MSD-10_030123A Prep Date: . 01/23/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual Benzene 9.95 0.5 10 100 80 120 Toluene 10.4 0.5 10 104 80 120 Ethylbenzene 10.4 0.5 10 104 80 120 m01�1 p-Xylene 20.6 0.5 20 103 73 129 lene10.3 0.5 10 103 73 127 : 3,2-Dichloroethane-d4 11 10 110 71 130 Surr.Toluene-d8 10.3 10 103 69 127 Surr:4-Bromofluorobenzene 10.1 10 101 80 123 Sample Matrix Spike Type MS Test Code: EPA Method SW8260B File ID: D:(HPCHEM\MS101DATA1030123103012311.D Batch ID: MSiOW0123A Analysis Date: 01/23/2003 11:25 Sample ID: 03012224-01AMS Units: pgIL Run ID:GC/MSD_10_030123A Prep Date: 01/23/2003 Anatyte Result PQL SpkVal SpkRefVal %REC LowLimit Hightimit RPD Ref Val %RPD Qual Benzene 48 1.3 50 0 96 80 120 Toluene 48.1 1.3 50 0 96 80 120 Ethylbenzene 51.7 1.3 50 0 103 80 120 m,p-Xylene 103 1.3 100 0 103 73 129 o-Xylene 52 1.3 50 0 104 73 127 Surr: 1,2-Dichloroethane-d4 55.1 50 110 71 130 Surr:Toluene-d8 48.9 50 98 69 127 Surr:4-Bromofluorobenzene 48.9 50 98 80 123 Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B File ID: D:IHPCHEMIMSIOIDATA1030123h03012312.D Batch ID: MSIOW0123A Analysis pate: 01/23/2003 11.47 Sample ID: 03012224-OIAMSD Units: liglL Run ID:GC/MSD-10-030123A Prep Date: 01/23/2003 Anafyte Result PQL SpkVal SpkRefVal %REC LowLimit Hightimit RPD Ref Val %RPD Qual Benzene 49 1.3 50 0 98 80 120 47.95 2.21 Toluene 48.9 1.3 50 0 98 80 120 48.09 1.61 Ethylbenzene 53 1.3 50 0 106 80 120 51.69 2.56 m,p-Xylene 108 1.3 100 0 108 73 129 103.1 4.28 o-Xylene 54.4 1.3 50 0 109 73 127 52.04 4.42 Surr: 1,2-Dichloroethane-d4 54.9 50 110 71 130 Surr:Toluene-d8 48.1 50 96 69 127 Surr:4-Bromofluorobenzene 48.6 50 97 80 123 ments: NO-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank.