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COLUMBIA ANALYTICAL SERVICES, INC. <br /> Analytical Report <br /> .Client: EMCON Service Request: 59901065 <br /> Project: USA Station No,65/Lodi,CA/20A41-008.001 Date Collected: 3130199 <br /> Sample Matrix: Water Date Received: 4/l/99 <br /> BTEX,MTBE and TPH as Gasoline <br /> Sample Name: S-2 Units: ug/L(ppb) <br /> Lab Code: 59901065-010 Basis: NA <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> TPH as Gasoline EPA 5030 CA/LUFT 50 40 NA 4/8/99 2300 <br /> Benzene EPA 5030 8020 0.5 20 NA 418/99 120 <br /> Toluene EPA 5030 8020 0.5 20 NA 4/8/99 5.5 <br /> Ethyibenzene EPA 5030 8020 0.5 20 NA 4/8/99 88 <br /> Xylenes,Total EPA 5030 8020 0.5 20 NA 4/8/99 270 <br /> Methyl 1er1-Butyl Ether EPA 5030 8020 3 40 NA 418199 2900 <br /> 3S22O20597p <br /> Page 17 <br />