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110'_ad Avenue South.kD7.Pacheco-('A <br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925-798-1622 <br /> Website:www.mccampbell,com E-mail,mam�nmrca;upbeltcom <br /> Advanced GeoEnvironmental, Inc. Client Project ID: National Freight Date Sampled: 12!17103 <br /> 837 Shaw Road Date Received: 12/18/03 <br /> Client Contact: Paul Dotson Date Extracted: 12/23/03-12/25/0-', <br /> Stockton. CA 95215 <br /> Client P.O.: Date Analyzed: 12123103-12125/03 <br /> Gasoline Range (C6-C12) Volatile Hydrocarbons as Gasoline with RTEX and MT141 * <br /> Extraction niethod: SW-5030B Analytical methods: SW8021B;80150m Work Order. 0312365 <br /> I-ab ID Client ID Matrix 1,P11(g) MTBE Benzene Toluene E,thylbenzene Xylenes DF SS <br /> 001A MWP121703 W 770,g,h,i --- NO ND ND Nl) 1 97.7 <br /> 002A M W2i 121703 W ND ND ND ND ND 1 532-1 <br /> 003A MW,.'12170', W ND,i --- ND ND ND ND 1 90.0 <br /> 004A MW4r121703 W NDJ --- ND ND ND ND 1 90.3 <br /> DOA MW5/121703 W NDJ ND ND ND ND 1 103 <br /> i <br /> i <br /> I <br /> Reporting Limit for DF=1: W 50 5.0 0.5 0.5 0.5 0.5 1 m-1- <br /> ND means not detected n or <br /> above the repomng limit S NA NA NA NA NA NA 1 mg/Kg <br /> water anti vapor samples and all TCLP&SPLP extracts are reported in ug l„soil.+sludge!solid samples in mg,,kg, wipe samples inµg;wipe, <br /> productrniI/non-aqueous liquid samples in mWL. <br /> 4 cluttered chromatogram;sample peak coelutes with surrogate peak. <br /> +The,allowing descriptions of the'I'Pll chromatogram are cursory in nature and McCampbell Analytical is not responsible for their interpretation:a) <br /> unmodified or weakly modified gasoline is significant;b)heavier gasoline range compounds are significant(aged gasoline?),c)lighter gasoline ranee <br /> compounds(the most mobile fraction)are significant;d)gasoline range compounds having broad chromatographic peaks are significant,biologically <br /> altered gasoline'?;e)TPH pattern that does not appear to be derived from gasoline(stoddard solvent/mineral spirit'?);t)one to a few isolated non-target <br /> peaks present;g)strongly aged gasoline or diesel range compounds are significant;h)lighter than water immiscible sheen/product is present;i)liquid <br /> sample that contains greater than--2 vol.%sediment;j)reporting limit raised due to high MTBE content;k)TPH pattern that does not appear to be <br /> derived from gasoline(aviation gas).m)no recognizable pattern. <br /> DHS Certification No. 1644 Angela Rydelius, Lab Manager <br />