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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax : 925-798-1622 <br /> http://www.mccampbell.co E-mail;main@mccampbell.com <br /> Advanced GeoEnvironmental Client Project ID: National Freight Date Sampled: 08114-08/15/00 <br /> 4005 North Wilson Way Date Received: 08/18/00 <br /> Stockton, CA 95205 Client Contact: Tim Cuellar Date Extracted: 08/18/00 <br /> + <br /> Client P.O: Date Analyzed: 08/21-08/22/00 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 45282 45283 45284 45285 <br /> Reporting Limit <br /> Client 1D MW3-15 MW3-30 MW3-40 MW3-50 <br /> Matrix S S S S S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND ND ND ND 5.0 i.0 <br /> Ethyl tert-Butyl Ether(ETSE) ND ND ND ND 5.0 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5.0 1.0 <br /> _ tert-Butanol ND ND ND ND 25 5.0 <br /> Methanol ND ND I ND ND 1 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromotluoromethane 1]11 7 113 114 112 <br /> Comments: <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit;N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than--5 vol.%sediment;6)sample diluted due to <br /> high organic content <br /> _. DHS Certification No. 1644 Edward Hamilton, Lab Director <br />