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I 10 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCA1VIPBELL ANALYTICAL INC. Telephone :925-798-1620 Fax : 925-798-1622 <br /> http://www.mccampbell.com E-mail:main @mccampbel1,com <br /> Advanced GeoEnvironmental Inc. Client Project ID: National Freight Inc. i Date Sampled: 08/23/00 <br /> 4005 N. Wilson Way Date Received: 08/29/00 <br /> Stockton.,CA 95205 Client Contact: Tim Cuellar Date Extracted: 08/29/00 <br /> Client P.O: Date Analyzed: 09101-09/06100 <br /> Oxygenated Volatile Organics By GUMS <br /> _ EPA method 8260 modified <br /> Lab ID 46[06 46107 46108 <br /> Reporting Limit <br /> Client ID MW-1108/23/00 MW-2/08/23/00 MW-3/08/23/00 <br /> Matrix W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND ND ND 5.0 1.0 <br /> Ethyl tert-Butyl Ether(ETBE) ND ND ND 5A 1.0 <br /> Methyl-tert Butyl Ether(MTBE) ND ND ND 5.0 1.0 <br /> tert-Amyl Methyl Ether(TAME) ND ND ND 5.0 1.0 <br /> tert-Butanol ND ND ND 25 5.0 <br /> Methanol ND ND ND 1000 200 <br /> Ethanol ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromoiluoromethane 102 97 90 <br /> Comments: i <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/STLC 1 SPLP extracts in ug/l. <br /> ND means not detected above the reporting limit;N/A means surrogate riot applicable to this analysis <br /> (h)lighter than water immiscible sheen is present;(i)liquid sample that contains greater than—5 vol.°','o sediment;(j)sample diluted due to <br /> high organic content <br /> DHS Certification No. 1644 t Edward Hamilton, Lab Director <br />