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Date: Al ha Analytical, Inc. - C SReport Work Or 08-Jan-01 p )' � `t Summary p O1016402G2 Method Blank Test Code: SW82608 Batch ID_ MS4W0104A Analysis Date:_01104/2001 12:24 Sample ID: MBLK MS4W0104A Units: NgIL Run ID: GCIMSD_4_010104 Prep Date: 01/04/2001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual rtiary Butyl Alcohol(TBA) ND 20 ethyl tent-butyl ether(MTBE) ND 0.5 Di-isopropyl Ether(D]PE) ND 1 Ethyl Tertiary Butyl Ether(ETBE) ND 1 Benzene NO 0.5 Tertiary Amyl Methyl Ether(TAME) NO 1 Toluene NO 0.5 Ethylbenzene ND 0.5 m,p-Xylene ND 0.5 o-Xylene ND 0.5 Ethanol ND 500 Laboratory Control Spike Test Code: SW82608 Batch ID: MS4W0104A Analysis Date: 01/0512001 01:16 Sample ID: LCS MS4W0104A Units: NgIL Run ID: GCIMSD_4_010104 Prep Date: 0110512001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Methyl tert-butyl ether(MTBE) 9.33 0.5 10 93 70 142 Benzene 10.2 0.5 10 102 76 127 Toluene 10.2 0.5 10 102 76 125 Ethylbenzene 10.1 0.5 10 101 64 132 m,p-Xyiene 21.3 0.5 20 107 70 130 o-Xylene 10.2 0.5 10 102 70 130 Sample Matrix Spike Test Code: SW82608 Batch ID. MS4W0104A Analysis Date: 01/05/2001 01:57 Sample ID: 01010202-10AMS Units: µ911- Run ID: GCIMSD_4_010104 Prep Date: 01/05/2001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Methyl tert-butyl ether(MTBE) 53.5 2.5 50 6.09 95 70 142 Benzene 52.5 2.5 50 0 105 76 127 Toluene 52.8 2.5 50 0 106 76 125 Ethylbenzene 52.7 2.5 50 0 105 64 132 m,p-Xylene 111 2.5 100 0.6 111 70 130 -o Xylene 53.4 2.5 50 0 107 70 130 Sample Matrix Spike Duplicate Test Code: SW8260B Batch ID: MS4W0104A Analysis Date: 01/05/2001 02:18 Sample ID: 01010202-10AMSD Units: pg1L Run ID: GC/MSD-4-010104 Prep Date: 01105!2001 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual Methyl tert-butyl ether(MTBE) 53.2 2.5 50 6.09 94 70 142 53.49 0.55 Benzene 51.4 2.5 50 0 103 76 127 52.47 2.14 Toluene 52.4 2.5 50 0 105 76 125 52.8 0.856 Ethylbenzene 51.5 2.5 50 0 103 64 132 52.67 2.19 m,p-Xylene 109 2.5 100 0.6 109 70 130 111.2 1.65 o-Xylene 52.6 2.5 50 0 105 70 130 53.37 1.47 Comments: NO-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank.