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Date. Work Order: IO-Jan-01 Alpha Analytical, Inc. - C Summa� Re ort 00122961 Method Blank Test Code: SW82608 Batch ID: MS9W0102A Analysis Date: 01/02/2001 13:36 Sample ID: MBLK MS9W0102AIB Units: pglL Run ID: GCIMSD_9_010102 Prep bate: 01/02/2001 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual ertiary Butyl Alcohol (TBA) ND 20 ethyl tert-butyl ether(MTBE) ND 0.5 Di-isopropyl Ether(DIPE) ND 1 Ethyl Tertiary Butyl Ether(ETRE) ND 1 Benzene ND 0.5 Tertiary Amyl Methyl Ether(TAME) ND 1 Toluene ND 0.5 Ethylbenzene ND 0.5 m,p-Xylene ND 0.5 o-Xylene ND 0.5 Ethanol ND 500 Laboratory Control Spike Test Code: SW8260B Batch ID: M59W0102A Analysis Date: 09/03/2001 02_04 Sample ID: LCS MS9W0102A Units: pg1L Run ID: GCIMSD_9_010102 Prep Date: 01/0312001 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Quat - Methyl tert-butyl ether(MTBE) 8.4 0.5 10 84 70 142 Benzene 8.39 0.5 10 84 76 127 Toluene 7.99 0.5 10 80 76 125 Ethylbenzene 8.13 0.5 10 81 64 132 m,p-Xylene 16.8 0.5 20 84 70 130 o-Xylene 8.38 0.5 10 84 70 130 Sample Matrix Spike Test Code: SW8260B Batch ID: MS9W0102A Analysis Date: 01103/2001 02:24 Sample ID: 00122961-02AMS Units: pg1L Run ID: GCIMSD_9_010102 Prep Date: 01/03/2001 Analyte Result PQL SpkVal SpkRefVal %REC LcwLimit HighLimit RPD Ref Val %RPD Qual Methyl tert-butyl ether(MTBE) 44.1 2.5 50 0 88 70 142 Benzene 42.1 2.5 50 0 84 76 127 Toluene 41.2 2.5 50 0.64 81 76 125 Ethylbenzene 41.3 2.5 50 0 83 64 132 m,p-Xylene 86 2.5 100 0 86 70 130 Xylene 42.9 2.5 50 0 86 70 130 ample Matrix Spike Duplicate Test Code: SW8260B Batch ID: M59W0102A Analysis Date: 01/03/2009 02:45 Sample ID: 00122961-02AMSD Units: pglL Run ID: GCIMSD_9_010102 Prep Date: 01/03/2001 Analyte Result PQL SpkVal SpkRefVat %REC LowLimit HighLimit RPD Ref Val %RPD Qual Methyl tert-butyl ether(MTBE) 41.1 2.5 50 0 82 70 142 44.05 7 Benzene 39.2 2.5 50 0 78 76 127 42.14 7.28 Toluene 39 2.5 50 0.64 77 76 125 41.17 5.61 Ethylbenzene 38.6 2.5 50 0 77 64 132 41.29 6.68 m,p-Xylene 80 2.5 100 0 80 70 130 86.01 7.23 o-Xylene 40.9 2.5 50 0 82 70 130 42.93 4.94 Comments: ND-Not Detected at the Reporting Limit. D-If the spiked value is<25%of the reference value,recovery should not be calculated. S-Spike Recovery outside accepted recovery limits. M-Spike Recovery outside accepted recovery limits due to matrix. B-Analyte detected in the associated Method Blank.