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I <br /> � r <br /> ATTACHMENT C <br /> FIELD AND LABORATORY PROCEDURES <br /> Chevron 9-6258, 2409 East Main Street at F Street, Stockton, CA <br /> by chain-of-custody documentation. The well casing will be surveyed to the nearest 0.01 feet <br /> in elevation to a known benchmark. <br /> Organic Vapor Procedures <br /> Soil samples collected during drilling will be analyzed in the field for ionizable organic <br /> compounds using an organic vapor meter (OVM) or a photo-ionization detector (PID) with a <br /> 10.2 eV lamp. The test procedure will involve measuring approximately 30 grams from an <br /> undisturbed soil sample, placing this subsample in a ziplock type bag or in a clean glass jar, <br /> and sealing the jar with aluminum foil secured under a ring-type threaded lid. The container <br /> will be warmed for approximately 20 minutes (in the sun), then the head-space within the <br /> container will be tested for total organic vapor, measured.in parts per million as benzene <br /> (ppm; volume/volume). The instrument will be calibrated prior to drilling using a 100-ppm <br /> isobutylene standard (in air) and a sensitivity factor of 55, which relates the photo-ionization <br /> potential of benzene to that of isobutylene at 100 ppm. The results of the field-testing will be <br /> noted on the boring logs. PID and OVM readings are useful for indicating relative levels of <br /> contamination, but cannot be used to evaluate hydrocarbon levels with the confidence of <br /> laboratory analyses. <br /> Laboratory Procedures <br /> Selected soil and groundwater samples collected will be analyzed for the presence of TPHg <br /> EPA Method 8015, and BTEX, and fuel oxygenates (MtBE, EtBE, TBA, TAME, DIPE, <br /> methanol, and ethanol) using EPA Method 826013. <br /> Soil Cuttings and Purge Water <br /> Soil cuttings generated during drilling operations will be temporarily stored on plastic or in <br /> DOT-approved 55-gallon drums pending transport by the disposal contractor to an <br /> appropriate disposal or treatment facility. A California=certified disposal contractor will <br /> remove contaminated soil cuttings to an appropriate disposal facility. - Water generated <br /> during steam cleaning and development of the new wells will be temporarily stored in DOT- <br /> approved 55-gallon drums pending transport by the disposal contractor to an appropriate <br /> disposal or treatment facility. <br />