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!!science <br /> nvironmental Quality Control -Spike/Spike Duplicate <br /> k ® aboratories, Inc. <br /> Kiff Analytical Date Received: 12/09/04 <br /> 2795 2nd Street, Suite 300 Work Order No: 04-12-0584 <br /> Davis, CA 95616-6593 Preparation: EPA 1311 <br /> Method: EPA 8270C <br /> Project Shell Station <br /> Date Date MS/MSD Batch <br /> Quality Control Sample ID Matrix Instrument Prepared Analyzed Number <br /> SPA Solid GC/MS Y 12/13/04 12/13/04 041213501 <br /> Parameter MS%REC MSD%REC %REC CL RPD RPD CL Qualifiers <br /> Phenol 45 44 20-120 3 0-42 <br /> 2-Chlorophenol 80 77 23-134 3 0-40 <br /> 1,4-Dichlorobenzene 88 85 20-124 4 0-28 <br /> N-Nitroso-di-n-propylamine 107 101 0-230 6 0-38 4 <br /> 1,2,4-Trichlorobenzene 79 76 44-142 4 0-28 <br /> Acenaphthene 90 87 47-145 3 0-31. <br /> 2,4-Dinitrotoluene 91 86 39-139 6 0-38 <br /> RPD-Relative Percent Difference, CL-Control Limit <br /> 7440 Lincoln Way, Garden Grove, CA 92841-1427 TEL:(714) 895-5494 FAX: (714)894-7501 <br /> i <br />