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10/25/2004 16:33 <br />Report # _ Q289-01 <br />20957"q16 <br />GEO <br />CERTIFICATE OF ANALYSIS <br />8260B <br />Sample ID: SR1/101404 Steam Rack Influent Sludge <br />Lab ID: Q201625 <br />PAGE 14/25 <br />Method RL Analyte Results Units <br />8260B 25 <br />Bromobenzene <br />ND pg/Kg <br />25 <br />Bromochloromethane <br />ND <br />25 <br />Bromomethane <br />ND <br />25 <br />n-Butylbenzene <br />ND <br />25 <br />sec-Butylbenzene <br />ND <br />25 <br />tert-Butylbenzene <br />ND <br />25 <br />Chloroethane <br />ND <br />50 <br />2-Chloroethylvinyl Ether <br />ND <br />25 <br />Chloromethane <br />ND <br />25 <br />2-Chlorotoluene <br />ND <br />25 <br />4-Chlorotoluene <br />ND <br />25 <br />Dibromomethane <br />ND <br />25 <br />1,3 -Dichlorobenzene <br />ND <br />25 <br />Dichlorodifluoromethane <br />ND <br />25 <br />1,3-Dichloropropane <br />ND <br />25 <br />2,2-Dichloropropane <br />ND <br />25 <br />1,1-Dichloropropene <br />ND <br />25 <br />Hexachlorobutadiene <br />ND <br />25 <br />Isopropylbenzene <br />ND <br />25 <br />p-Isopropyltoluene <br />158 <br />25 <br />Methyl tert-Butyl Ether (MTBE) <br />ND <br />25 <br />n-Propylbenzene <br />499 <br />25 <br />1,1,1,2 -Tetrachloroethane <br />ND <br />25 <br />1,2,3-Trichlorobenzene <br />ND <br />25 <br />1,2,3-Trichloropropane <br />ND <br />100 <br />1,2,4-Trimethylbenzene <br />3070 <br />100 <br />1,3,5-Trimethylbenzene <br />919 <br />25 <br />1,2-Dibromo-3-chloropropant,(DBCP) <br />ND <br />Surrogate Amnt Spiked <br />1,2-Dichloroethane-d4 100 <br />2-Bromo-l-chloropropane 100 <br />4-Bromofluorobenzene 100 <br />* Surrogate criteria not met due to high level of analyte concentration <br />Mano D'of io <br />Chemist <br />Certification # 1157 <br />Page 2 of 2 <br />Amnt Recovered % Recovery <br />174* 174.00 <br />233* 233.00 <br />220* 220.00 <br />QC Limit % <br />66-133 <br />63-139 <br />64-136 <br />Donna Keller <br />Laboratory Director <br />