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'ERTIFICATE OF ANALYSIS <br />8260B <br />Report # Q289-01 <br />Sample ID: HT1/101404 Process Tank Sludge <br />Lab ID: Q201624 <br />Method RL Analyte Results Units <br />8260B 5.0 <br />Bromobenzene <br />ND µg/Kg <br />5.0 <br />Bromochloromethane <br />ND <br />5.0 <br />Bromomethane <br />ND <br />5.0 <br />n-Butylbenzene <br />ND <br />5.0 <br />sec-Butylbenzene <br />ND <br />5.0 <br />tert-Butylbenzene <br />ND <br />5.0 <br />Chloroethane <br />ND <br />10 <br />2-Chloroethylvinyl Ether <br />ND <br />5.0 <br />Chloromethane <br />ND <br />5.0 <br />2-Chlorotoluene <br />ND <br />5.0 <br />4-Chlorotoluene <br />ND <br />5.0 <br />Dibromomethane <br />ND <br />5.0 <br />1,3 -Dichlorobenzene <br />ND <br />5.0 <br />Dichlorodifluoromethane <br />ND <br />5.0 <br />1,3-Dichloropropane <br />ND <br />5.0 <br />2,2-Dichloropropane <br />ND <br />5.0 <br />1,1-Dichloropropene <br />ND <br />5.0 <br />Hexachlorobutadiene <br />ND <br />5.0 <br />Isopropylbenzene <br />ND <br />5.0 <br />p-Isopropyltoluene <br />6.9 <br />5.0 <br />Methyl tert-Butyl Ether (MTBE) <br />ND <br />5.0 <br />n-Propylbenzene <br />ND <br />5.0 <br />1,1,1,2 -Tetrachloroethane <br />ND <br />5.0 <br />1,2,3-Trichlorobenzene <br />ND <br />5.0 <br />1,2,3-Trichloropropane <br />ND <br />5.0 <br />1,2,4-Trimethylbenzene <br />37 <br />5.0 <br />1,3,5-Trimethylbenzene <br />16 <br />5.0 <br />1,2-Dibromo-3-chloropropane(DBCP) <br />ND <br />6aio D Unoffio <br />Chemist <br />Surrogate <br />Amnt Spiked <br />Amnt Recovered <br />% Recovery <br />QC Limit % <br />1,2-Dichloroethane-d4 <br />20 <br />24.1 <br />120.50 <br />66-133 <br />2-Bromo-l-chloropropane <br />20 <br />23.1 <br />115.50 <br />63-139 <br />4-Bromofluorobenzene <br />20 <br />15.2 <br />76.00 <br />64-136 <br />Certification # 1157 <br />Page 2 of 2 <br />Donna Keller <br />Laboratory Director <br />