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Ge*Analytical Laboratories, Inc. <br />1405 Kansas Avenue Modesto CA 95351 Phone (209) 572-0900 Fax (209) 572-0916 <br />Report # Q289-01 <br />San Joaquin County <br />304 E. Weber 3rd Floor <br />Stockton CA 95202 <br />CERTIFICATE OF ANALYSIS Date: 11/01/04 <br />8270C TCLP , <br />Project: Cherokee Main <br />PO# <br />Sample ID: SR2/101404 Steam Rack Effluent <br />Lab ID: Q307094 <br />Date Rec d: 10/15/04 <br />Date Started: 10/28/04 <br />Date Completed:10/30/04 <br />Date Sampled: 10/14/04 <br />Time: <br />Sampler <br />Method RL <br />Analyte <br />Results Units <br />8270C TCLP 0.02 <br />o -Cresol (2-methylphenol) <br />ND mg/L <br />0.02 <br />m -Cresol (3-methylphenol) <br />ND <br />0.02 <br />p -Cresol (4-methylphenol) <br />ND <br />0.02 <br />Cresol <br />ND <br />0.02 <br />2,4,5 -Trichlorophenol <br />ND <br />0.02 <br />2,4,6 -Trichlorophenol <br />ND <br />0.10 <br />Pentachlorophenol <br />ND <br />0.02 <br />1,4-Didilorobenzene <br />ND <br />0.02 <br />2,4-Dinitrotoluene <br />ND <br />0.02 <br />Hexachlorobenzene <br />ND <br />0.02 <br />Hexachlorobutadiene <br />ND <br />0.02 <br />Hexachloroethane <br />ND <br />0.02 <br />Nitrobenzene <br />ND <br />0.02 <br />Pyridine <br />ND <br />Gregory Merciadis <br />Chemist <br />I <br />Surrogate <br />Nitrobenzene -d5 <br />2-Fluorobiphenyl <br />Terphenyl-d„ <br />2 -fluorophenyl <br />Phenol -d5 <br />2,4,6-Tbromophenol <br />Certification # 1157 <br />Amnt Spiked Amnt Rec. % Recovery QC Limit % <br />100 <br />58.38 <br />58.4 <br />35-114 <br />100 <br />122.03 <br />122.0 <br />43-141 <br />100 <br />119.83 <br />119.8 <br />33-141 <br />150 <br />127.08 <br />84.7 <br />21-100 <br />150 <br />97.42 <br />64.9 <br />10-94 <br />150 <br />156.30 <br />104. <br />10-123 <br />v <br />Donna Keller <br />Laboratory Director <br />