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EXCELCHE <br /> ENVIRONMENTAL LABS <br /> 500 Giuseppe Court, Suite 9 a <br /> Roseville, CA 95678 <br /> ' Phone# (916) 773-3664 Fax# (916) 773-4784 <br /> ANALYSIS REPORT <br /> Attention Mr Bill Welter Date Sampled 05/30/96 <br /> LUSH GEOSCIENCES Date Received 05/30/95 <br /> t 3560 Business Drive, Suite 120 <br /> Sacramento, CA 95816 <br /> Protect 524-001 / Marci's Diesel Matrix Soil <br /> l <br /> Sample ! b LB-1-12 Sample E D LB-1-14 Sample I D LB-1-16 <br /> Lab I D S0596378 Lab I D S0596379 Lab I D 50596380 <br /> ' Analyte ppm (mg/kg) ppm (mg/kg) ppm (mg/kg) <br /> 3 Results R L Analysis Date Results R L Analysis Dale Results R L Analysis Date <br /> Benzene ND 1 23 6/5196 ND 1 26 6/6/96 ND 02 6/6196 <br /> Toluene ND 1 23 6/5/96 ND 1 26 6/6/96 ND 026 616196 <br /> Ethylbenzene ND 1 23 615196 2 34 1 26 6/6/96 ND 026 6/6/96 <br /> Total Xylenes 254 1 23 6/5/96 411 1 26 616196 0 32 026 616196 <br /> TPH as Gasoline 396 1231 615196 800 126 616196 674 1 26 Oj 616196 <br /> TPH as Diesel 1 16600 148 6/5/961 64500 520 6/5/9150L_6220 1 100 615196 <br /> j' Sample I D LB-1-18 Sample I D LB-1-20 Sample I D LB-1-21 <br /> Lab I D 50596381 Lab I D S0596382 Lab I D S0596383 <br /> Analyte ppm (mg/kg) ppm (mglkg) ppm (mg/kg) <br /> ' Results R L Ana"is Date Results R L Analysts Date Results R L Analysis Date <br /> Benzene ND 0 51 616196 ND 1 30 616196 ND 0 13 616196 <br /> Toluene ND 0 51 616196 ND 1 30 6/6196 ND 0 13 616196 <br /> ' Ethylbenzene ND 0 51 6/6/96 ND 1 30 6/6/96 ND 0 13 616196 <br /> Total Xylenes ND 0 51 616196 1 60 1 30 616196 ND 0 13 616/96 <br /> TPH as Gasoline 727 1 51 01 6/6/96 141 130 6/6/96 ND 1301 6/6196 <br /> ' TPH as Diesel 3480 1 100 6/5/9E31 18000 100 6/5/96 26 5 1 01 6/5196 <br /> ppm=parts per million=milligram per kilogram <br /> R L =Reporting Limit <br /> ND=Not Detected Compound's)may be present at concentrations below the reporting limit <br /> Analytical Procedures <br /> BTEX-Benzene Toluene Ethylbenzene Total Xylene Isomers are measured by extraction using EPA Method 5030 followed by <br /> ' analysis using EPA Method 8020 which utilizes a gas chromatograph(GC)equipped with a photoionizatlon detector <br /> TPHg Total petroleum hydrocarbons as gasoline(low-to-medium boiling points)are analyzed using modified EPA Method 8015 <br /> which utilizes a gas chromatograph(GC)equipped with a flame Ionization detector(FID) <br /> ' <br /> 06/11/96 <br /> laboratory Representative Date Reported <br /> ' EXCELCHEMI ENVIRONMENTAL LABS IS CERTIFIED BY THE STATE OF CALIFORNIA OEPARTPIENT OF HEALTH SERVICES ASA HAZARDOUS WASTE TESTING LABORATORY <br /> (Certification Nos 1750 2119) <br />