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Entech Analytical Labs, Inc. <br /> 3334 Victor Court • Santa Clara, CA 95054 • (408) 588-0200 • Fax (408) 588-0201 <br /> Compliance& Closure, Inc Date 12/12/00 <br /> 7020 Koll Center Parkway, Suite 134 Date Received 12/1/00 <br /> Pleasanton, CA 94566-3107 Protect Name Quick Stop#121 <br /> Project Number 12118-5 <br /> Attn Gary Mulkey P 0 Number <br /> Sampled By Client <br /> Certified Analytical Report <br /> Order ID 23417 Lab Sample ID 23417-003 Client Sample ID RW-1@15 <br /> Sample Time 9 10 AM Sample Date 11/30/00 Matrix Solid <br /> Parameter Result Flag DF PQL, „"DLR Units Analysis Date QC Batch ID Method <br /> Dusopropyl Ether ND 500 5 2500 pg/Kg 1218!00 SMS1001207 EPA 8260B <br /> Ethyl-t-butyl Ether ND 500 5 2500 gglKg 1218/00 SMS1001207 EPA 8260B <br /> Methyl-t-butyl Ether 45000 500 5 2500 pg/Kg 12/8100 SMS 1001207 EPA 8260B <br /> tert-Amyl Methyl Ether ND 500 5 2500 jig/Kg 12/8/00 SMS1001207 EPA 8260B <br /> tert-Butanol ND 500 20 10000 pg/Kg 12/8/00 SMS1001207 EPA 8260B <br /> Surrogate Surrogate Recovery Control Limits{%} <br /> 4-BromoFluorobenzene 103 65 - 135 <br /> Dtbromofluoromethane 110 65 135 <br /> Toluene-d8 111 65 - 135 <br /> DF=Dilution Factor ND=Not Detected DLR=Detection Limit Reported PQL=Practical Quantitation Limit <br /> Analysis performed by Entech Analytical Labs Inc (CA FLAP 02346) <br /> Mt hell nderson, Laboratory DlrectorEnvlronmental Analy515 Since 1983 Page 3 of 6 <br />